3,4-二羟基苯甲酸甲酯合成路线 (共 60 条)
反应条件
sodium hydride in tetrahydrofuran T=0°C;
参考文献
Piguel, Sandrine; Ulibarri, Gerardo; Grierson, David S.
Tetrahedron Letters, 1999 , vol. 40, # 2 p. 291 - 294
反应条件
manganese(IV) oxide; acetic acid in methanol; water 0.666667 h;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 42 p. 8076 - 8078
反应条件
triethylamine T=20°C; 18 h;
参考文献
Delfourne, Evelyne; Despeyroux, Pierre; Gorrichon, Liliane; Veronique, Jacqueline
Journal of Chemical Research, Miniprint, 1991 , # 3 p. 532 - 544
反应条件
water; oxygen; copper; Cu2Cl2 1.) CH3CN; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 23, # 15 p. 1577 - 1580
反应条件
manganese(IV) oxide; water 2 h; Title compound not separated from byproducts.;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 42 p. 8076 - 8078
反应条件
1: 714 mg / diethyl ether 2: 44 mg / benzene / 20 h / 60 °C 3: 32 mg / 80percent AcOH / 1 h / Ambient temperature View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 29, # 10 p. 2893 - 2898
反应条件
methanol; potassium carbonate T=150 - 170°C; im geschlossenen Rohr;
参考文献
Chemische Berichte, , vol. 11, p. 133
反应条件
acetic acid 1 h; Ambient temperature;
参考文献
Ikeya, Yukinobu; Taguchi, Heihachiro; Yoshioka, Itiro
Chemical & Pharmaceutical Bulletin, 1981 , vol. 29, # 10 p. 2893 - 2898
反应条件
sodium peroxynitrite in phosphate buffer T=20 - 25°C; Nitration; hydroxylation; pH=7.0; Kinetics; Further Variations:Solvents;
参考文献
Tetrahedron Letters, , vol. 40, # 38 p. 6933 - 6937
反应条件
1: 50 percent / Amberlite IR 120 / 1.5 h / Heating 2: Et3N / 18 h / 20 °C View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 3 p. 532 - 544