3,5-二羟基苯甲酸甲酯合成路线 （共 124 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=75°C; 8 h;
参考文献
Percec, Virgil; Peterca, Mihai; Sienkowska, Monika J.; Ilies, Marc A.; Aqad, Emad; Smidrkal, Jan; Heiney, Paul A.
Journal of the American Chemical Society, 2006 , vol. 128, # 10 p. 3324 - 3334
反应条件
potassium carbonate in acetone Benzylation; 5 h; Heating;
参考文献
Maekelae, Taru; Matikainen, Jorma; Waehaelae, Kristiina; Hase, Tapio
Tetrahedron, 2000 , vol. 56, # 13 p. 1873 - 1882
反应条件
ammonium chloride in N,N-dimethyl-formamide
参考文献
Eli Lilly and Company Limited
Patent: US5863947 A1, 1999 ;
反应条件
1: 80 percent / potassium iodide; potassium carbonate; [18]crown-6 / acetone / 12 h / Heating 2: 98 percent / LiAlH4 / tetrahydrofuran / 6.5 h / 0 - 20 °C 3: 88 percent / carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 1 h / 20 °C 4: 85 percent / potassium iodide; potassium carbonate; [18]crown-6 / acetone / 10 h / Heating 5: 94 percent / LiAlH / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 13, # 12 p. 3346 - 3353
反应条件
1: potassium carbonate / acetonitrile / 20 °C 2: sodium hydroxide / 1,4-dioxane / 5 h / 20 °C View Scheme
参考文献
Song, Yu Min; Ha, Young Mi; Kim, Jin-Ah; Chung, Ki Wung; Uehara, Yohei; Lee, Kyung Jin; Chun, Pusoon; Byun, Youngjoo; Chung, Hae Young; Moon, Hyung Ryong
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 24 p. 7451 - 7455
反应条件
potassium carbonate in acetone
参考文献
Hotta, Hiroki; Kang, Soonchul; Umeyama, Tomokazu; Matano, Yoshihiro; Yoshida, Kaname; Isoda, Seiji; Imahori, Hiroshi
Journal of Physical Chemistry B, 2005 , vol. 109, # 12 p. 5700 - 5706
反应条件
1: potassium carbonate / acetonitrile / 20 °C 2: sodium hydroxide / 1,4-dioxane / 5 h / 20 °C 3: triethylamine; diphenyl phosphoryl azide / 80 °C 4: sodium hydroxide; benzoic acid / tetrahydrofuran / 0.5 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 24 p. 7451 - 7455
反应条件
potassium carbonate in N,N-dimethyl-formamide T=60°C;
参考文献
Luscombe, Christine K.; Proemmel, Steffen; Huck, Wilhelm T. S.; Holmes, Andrew B.; Fukushima, Hitoshi
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5505 - 5513
反应条件
18-crown-6 ether; potassium carbonate in acetone T=60°C; 36 h;
参考文献
Macromolecules, , vol. 38, # 15 p. 6276 - 6284
反应条件
18-crown-6 ether; potassium carbonate T=75°C; Williamson esterification; 24 h;
参考文献
Elmer, Stephanie L.; Zimmerman, Steven C.
Journal of Organic Chemistry, 2004 , vol. 69, # 21 p. 7363 - 7366
