Fmoc-l-alpha-苯丙氨醇合成路线 (共 5 条)
反应条件
12-molybdophosphoric acid HPMo; silica gel in dichloromethane T=20°C; 4 h; chemoselective reaction;
参考文献
Kumar, Ponminor Senthil; Kumar, Gaddale Devanna Kishore; Baskaran, Sundarababu
European Journal of Organic Chemistry, 2008 , # 36 p. 6063 - 6067
反应条件
sodium hydrogencarbonate in 1,4-dioxane; water T=20°C;
参考文献
Journal of the American Chemical Society, , vol. 128, # 12 p. 4023 - 4034
反应条件
1: With 4-methyl-morpholine; chloroformic acid ethyl ester in tetrahydrofuran T=-10°C; 0.166667 h; 2: With sodium tetrahydroborate in tetrahydrofuran 3: With water in tetrahydrofuran
参考文献
Journal of Organic Chemistry, , vol. 74, # 15 p. 5260 - 5266
反应条件
in 1,4-dioxane; water T=20°C; 16 h;
参考文献
Crestey, Francois; Ottesen, Lars K.; Jaroszewski, Jerzy W.; Franzyk, Henrik
Tetrahedron Letters, 2008 , vol. 49, # 41 p. 5890 - 5893
反应条件
sodium tetrahydroborate in tetrahydrofuran; water cooling;
参考文献
Babu, Vommina V. Suresh; Kantharaju; Sudarshan, Naremaddepalli S.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 8 p. 1880 - 1886