2-(N-异丁氧基甲酰胺基)乙烷基异氰合成路线 （共 3 条）
反应条件
1: With triethylamine; trichlorophosphate in dichloromethane 0.5 h; ice bath; 2: With potassium carbonate in dichloromethane 0.5 h;
参考文献
Xu, Ping; Zhang, Ting; Wang, Wenhao; Zou, Xiaomin; Zhang, Xin; Fu, Yiqiu
Synthesis, 2003 , # 8 p. 1171 - 1176
反应条件
1.1: 75 percent / tetrahydrofuran / 24.5 h / 0 - 20 °C 2.1: 90 percent / DCC / CH2Cl2 / 20 °C 3.1: POCl3; Et3N / CH2Cl2 / 0.5 h / ice bath 3.2: 68 percent / aq. K2CO3 / CH2Cl2 / 0.5 h View Scheme
参考文献
Xu, Ping; Zhang, Ting; Wang, Wenhao; Zou, Xiaomin; Zhang, Xin; Fu, Yiqiu
Synthesis, 2003 , # 8 p. 1171 - 1176
反应条件
1.1: 90 percent / DCC / CH2Cl2 / 20 °C 2.1: POCl3; Et3N / CH2Cl2 / 0.5 h / ice bath 2.2: 68 percent / aq. K2CO3 / CH2Cl2 / 0.5 h View Scheme
参考文献
Xu, Ping; Zhang, Ting; Wang, Wenhao; Zou, Xiaomin; Zhang, Xin; Fu, Yiqiu
Synthesis, 2003 , # 8 p. 1171 - 1176
