氧代[二(三氟甲基)]铵合成路线 (共 181 条)
反应条件
in tetrachloromethane
参考文献
Banks,R.E. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 1951 - 1957
反应条件
various ratios, room temp.;
参考文献
Gmelin Handbook: Sb: Org.Comp.1, 1.1.1.1.3, page 33 - 37
反应条件
2-lt;5,5-dimethyl-3,3-bis(trifluoromethyl)-1-pyrazolin-1-yliogt;-1,1,1,3,3,3-hexafluoropropan-2-ide 288 h; Ambient temperature; Further byproducts given;
参考文献
Journal of Fluorine Chemistry, , vol. 66, # 3 p. 279 - 286
反应条件
2-lt;5,5-dimethyl-3,3-bis(trifluoromethyl)-1-pyrazolin-1-yliogt;-1,1,1,3,3,3-hexafluoropropan-2-ide 288 h; Ambient temperature; Further byproducts given;
参考文献
Journal of Fluorine Chemistry, , vol. 66, # 3 p. 279 - 286
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 406 - 409
反应条件
17 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 406 - 409
反应条件
264 h; Ambient temperature; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 406 - 409
反应条件
bis(trimethylsilyl)methane 4 h; Ambient temperature; Further byproducts given;
参考文献
Ducker, Graham E.; Tipping, Anthony E.
Journal of Fluorine Chemistry, 1994 , vol. 66, # 3 p. 253 - 262
反应条件
4 h; Ambient temperature; Further byproducts given;
参考文献
Ducker, Graham E.; Tipping, Anthony E.
Journal of Fluorine Chemistry, 1994 , vol. 66, # 3 p. 253 - 262
反应条件
in further solvent(s) solvent: Cl2CFCF2Cl; sealed tube, -70°C for 1 d, shaking at room temp. for 20 min, left standing for another d; recrystn. from petroleum ether;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 5.2.3, page 87 - 96