氧代[二(三氟甲基)]铵合成路线 (共 181 条)
反应条件
stibine to (CF3)2NO is 1:2, -74°C, 1 h;
参考文献
Gmelin Handbook: Sb: Org.Comp.1, 1.1.1.1.3, page 33 - 37
反应条件
molar ratio 1:1, heating at 98°C 60 h, then trapped at -89°C;
参考文献
Ang, H. G.; Lien, W. S.
Journal of Fluorine Chemistry, 1978 , vol. 11, p. 419 - 432
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Gmelin Handbook: F: PerFHalOrg.SVol.1, 5.3.4, page 166 - 166
参考文献
Fisher, Raymond; Haszeldine, Robert N.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 406 - 409
参考文献
Banks,R.E. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 1951 - 1957
参考文献
Banks, R. E.; Haszeldine, R. N.; Stephens, C. W.
Tetrahedron Letters, 1972 , p. 3699 - 3701
反应条件
2160 h; Ambient temperature; KineticsRate constant;
参考文献
Anpo, M.; Chatgilialoglu, C.; Ingold, K.U.
Journal of Organic Chemistry, 1983 , vol. 48, # 22 p. 4104 - 4106
参考文献
ANG, H. G.; SO, K. K.
Journal of Fluorine Chemistry, 1982 , vol. 21, p. 221 - 242
反应条件
2-lt;5,5-dimethyl-3,3-bis(trifluoromethyl)-1-pyrazolin-1-yliogt;-1,1,1,3,3,3-hexafluoropropan-2-ide
288 h; Ambient temperature; Further byproducts given;
参考文献
Bell, David; Tipping, Anthony E.
Journal of Fluorine Chemistry, 1994 , vol. 66, # 3 p. 279 - 286
参考文献
Banks, Ronald E.; Birchall, J. Michael; Haszeldine, Robert N.; Hughes, Raymond A.; Nona, Shmaiel N.; Stephens, Christopher W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 455 - 456
反应条件
thiophosgene
-23 deg C , 4 h, then rt.;
参考文献
Booth, B. L.; Browne, R. F.; Haszeldine, R. N.; Varley, J. S.
Journal of Fluorine Chemistry, 1984 , vol. 24, p. 485 - 502