氧代[二(三氟甲基)]铵合成路线 (共 181 条)
反应条件
allyl bromide 168 h; Ambient temperature; Further byproducts given;
参考文献
Newsholme, Gordon; Tipping, Anthony E.
Journal of Fluorine Chemistry, 1994 , vol. 69, # 2 p. 163 - 170
反应条件
168 h; Ambient temperature; Further byproducts given;
参考文献
Newsholme, Gordon; Tipping, Anthony E.
Journal of Fluorine Chemistry, 1994 , vol. 69, # 2 p. 163 - 170
反应条件
bis(trimethylsilyl)methane 4 h; Ambient temperature; Further byproducts given;
参考文献
Journal of Fluorine Chemistry, , vol. 66, # 3 p. 253 - 262
反应条件
4 h; Ambient temperature; Further byproducts given;
参考文献
Journal of Fluorine Chemistry, , vol. 66, # 3 p. 253 - 262
反应条件
in neat (no solvent) byproducts: (CF3)2NOH; starting compds. mixture, cooled to -196°C under vacuum, allowing to warm to -78°C, keeping at -78°C for 10 min; vac. evapn., not isolated, detected by IR;
参考文献
Booth, Brian L.; Haszeldine, Robert N.; Holmes, Robert G.G.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1982 , p. 523 - 530
反应条件
KBrO3; sulfuric acid in water
T=21°C; 1 h; further reagents, solvents, reaction times, temperatures; Product distribution;
参考文献
Booth, Brian L.; Kosinski, Edward D.; Varley, John S.
Journal of Fluorine Chemistry, 1987 , vol. 37, p. 419 - 428
反应条件
lithium salt of 2-nitropropane in 1,2,2-trifluoro-trichloroethane
T=20°C;
参考文献
Zhao, Cheng-Xue; Jiang, Xi-Kui; Chen, Guo-Fei; Qu, Yan-Ling; Wang, Xian-Shan; Lu, Jian-Ying
Journal of the American Chemical Society, 1986 , vol. 108, # 11 p. 3132 - 3133
反应条件
in 1,2,2-trifluoro-trichloroethane
T=20°C;
参考文献
Zhao, Cheng-Xue; Jiang, Xi-Kui; Chen, Guo-Fei; Qu, Yan-Ling; Wang, Xian-Shan; Lu, Jian-Ying
Journal of the American Chemical Society, 1986 , vol. 108, # 11 p. 3132 - 3133
反应条件
in 1,2,2-trifluoro-trichloroethane
T=20°C;
参考文献
Zhao, Cheng-Xue; Jiang, Xi-Kui; Chen, Guo-Fei; Qu, Yan-Ling; Wang, Xian-Shan; Lu, Jian-Ying
Journal of the American Chemical Society, 1986 , vol. 108, # 11 p. 3132 - 3133
反应条件
in 1,2,2-trifluoro-trichloroethane
T=20°C;
参考文献
Zhao, Cheng-Xue; Jiang, Xi-Kui; Chen, Guo-Fei; Qu, Yan-Ling; Wang, Xian-Shan; Lu, Jian-Ying
Journal of the American Chemical Society, 1986 , vol. 108, # 11 p. 3132 - 3133