反应条件
1.1: n-butyllithium / tetrahydrofuran / 0.25 h / -78 °C 1.2: -78 - 20 °C 2.1: copper / N,N-dimethyl-formamide / 48 h / 80 °C 3.1: trichlorophosphate / 18 h / 150 °C 4.1: potassium hydroxide / 72 h / 100 °C 5.1: ammonium acetate / 4 h / 160 °C View Scheme
参考文献
Subasinghe, Nalin L.; Lanter, James; Markotan, Thomas; Opas, Evan; McKenney, Sandra; Crysler, Carl; Hou, Cuifen; O'Neill, John; Johnson, Dana; Sui, Zhihua
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 4 p. 1063 - 1069