1: KOH; PhOH / 2 h / 140 °C
2: NH4OAc / 14 h / 150 °C
3: pyridine / 1 h / 125 °C
4: n-BuLi / tetrahydrofuran / 0.5 h / -78 °C
5: NaBH4 / tetrahydrofuran; methanol / 0.08 h / 20 °C
View Scheme
参考文献
Rewinkel; Lucas; Smit; Noach; Van Dinther; Rood; Jenneboer; Van Boeckel
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 19 p. 2837 - 2842
1: KOH; PhOH / 2 h / 140 °C
2: NH4OAc / 14 h / 150 °C
3: pyridine / 1 h / 125 °C
4: n-BuLi / tetrahydrofuran / 0.5 h / -78 °C
5: NaBH4 / tetrahydrofuran; methanol / 0.08 h / 20 °C
6: Et3N / CH2Cl2 / 2 h / 20 °C
7: LiCl / tetrahydrofuran / 16 h / 20 °C
View Scheme
参考文献
Rewinkel; Lucas; Smit; Noach; Van Dinther; Rood; Jenneboer; Van Boeckel
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 19 p. 2837 - 2842
