1,3-二氯-5-乙烯基苯合成路线 （共 6 条）
反应条件
2,6-dimethylpyridine
T=25°C; 3 h;
参考文献
Shimizu, Nobujiro; Watanabe, Sin-ichiro; Hayakawa, Fumie; Yasuhara, Sigefumi; Tsuno, Yuho; Inazu, Takahiko
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 2 p. 500 - 504
反应条件
2: 97.6 percent / Sodium azide / acetone; H2O / 12 h / Ambient temperature
3: 2.4 percent / 650 °C / 10 - 15 Torr
View Scheme
参考文献
Abramovitch, Rudolph A.; Holcomb, William D.; Thompson, W. Marshall; Wake, Shigeo
Journal of Organic Chemistry, 1984 , vol. 49, # 26 p. 5124 - 5131
参考文献
Shimizu, Nobujiro; Watanabe, Shin-ichiro; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 7 p. 2249 - 2254
反应条件
1: 92 percent / diethyl ether / Ambient temperature
2: pyridine / diethyl ether
3: 90 percent aq. dioxane / 25 °C
View Scheme
参考文献
Shimizu, Nobujiro; Watanabe, Shin-ichiro; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 7 p. 2249 - 2254
反应条件
1: pyridine / diethyl ether
2: 90 percent aq. dioxane / 25 °C
View Scheme
参考文献
Shimizu, Nobujiro; Watanabe, Shin-ichiro; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 7 p. 2249 - 2254
反应条件
1,4-dioxane
T=25°C; ΔH(excit.)298, ΔS(excit.)298; β-silicon effect in solvolysis; other temperatures; other solvents; or base; Rate constantThermodynamic dataMechanism;
参考文献
Shimizu, Nobujiro; Watanabe, Shin-ichiro; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 7 p. 2249 - 2254
