(E)-1,3-二(4-甲基苯基)丙-2-烯-1-酮合成路线 （共 13 条）
反应条件
sodium hydroxide 0.0833333 h; Ambient temperature; Product distribution;
参考文献
Toda, Fumio; Tanaka, Koichi; Hamai, Koki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 3207 - 3209
反应条件
[Ir2(COD)2(SnCl3)2(Cl)2(μ-Cl)2] in 1,2-dichloro-ethane T=80°C; 0.75 h; Inert atmosphere;
参考文献
Chatterjee, Paresh Nath; Roy, Sujit
Tetrahedron, 2012 , vol. 68, # 19 p. 3776 - 3785
反应条件
FeCl3·6H2O in toluene T=80°C; 2 h; chemoselective reaction;
参考文献
Wang, Jialiang; Huang, Wen; Zhang, Zhengxing; Xiang, Xu; Liu, Ruiting; Zhou, Xigeng
Journal of Organic Chemistry, 2009 , vol. 74, # 9 p. 3299 - 3304
反应条件
samarium (III) iodide in tetrahydrofuran T=20°C; 3 h;
参考文献
Fan, Xuesen; Zhang, Yongmin
Journal of Chemical Research - Part S, 2002 , # 9 p. 439 - 441
反应条件
1: methanol; sodium tetrahydroborate / 2 h / 0 - 10 °C / Inert atmosphere 2: [Ir2(COD)2(SnCl3)2(Cl)2(μ-Cl)2] / 1,2-dichloro-ethane / 0.75 h / 80 °C / Inert atmosphere View Scheme
参考文献
Chatterjee, Paresh Nath; Roy, Sujit
Tetrahedron, 2012 , vol. 68, # 19 p. 3776 - 3785
反应条件
1: sodium hydroxide / ethanol; water / 4 h / 0 - 20 °C / Inert atmosphere 2: methanol; sodium tetrahydroborate / 2 h / 0 - 10 °C / Inert atmosphere 3: [Ir2(COD)2(SnCl3)2(Cl)2(μ-Cl)2] / 1,2-dichloro-ethane / 0.75 h / 80 °C / Inert atmosphere View Scheme
参考文献
Chatterjee, Paresh Nath; Roy, Sujit
Tetrahedron, 2012 , vol. 68, # 19 p. 3776 - 3785
反应条件
1: sodium hydroxide / ethanol; water / 4 h / 0 - 20 °C / Inert atmosphere 2: methanol; sodium tetrahydroborate / 2 h / 0 - 10 °C / Inert atmosphere 3: [Ir2(COD)2(SnCl3)2(Cl)2(μ-Cl)2] / 1,2-dichloro-ethane / 0.75 h / 80 °C / Inert atmosphere View Scheme
参考文献
Chatterjee, Paresh Nath; Roy, Sujit
Tetrahedron, 2012 , vol. 68, # 19 p. 3776 - 3785
反应条件
pyridine; hydroxylamine hydrochloride in water 4 h; Heating;
参考文献
Elkasaby, M. A.; Salem, M. A. I.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 7 p. 571 - 575
反应条件
potassium carbonate 0.075 h; Microwave irradiationSonicationReflux;
参考文献
Tetrahedron Letters, , vol. 53, # 9 p. 1160 - 1162
反应条件
bismuth trifluoromethanesulphonate; malononitrile in dichloromethane T=20°C; 15 h; regioselective reaction;
参考文献
Shang, Jun-Yan; Li, Fei; Bai, Xing-Feng; Jiang, Jian-Xiong; Yang, Ke-Fang; Lai, Guo-Qiao; Xu, Li-Wen
European Journal of Organic Chemistry, 2012 , # 14 p. 2809 - 2815
