3,5-二甲基-4-甲氧基苯甲酸合成路线 （共 7 条）
反应条件
1: With sodium hydroxide in ethanol T=120°C; pressure reactor; 2: With hydrogenchloride in water
参考文献
Almirall, S.A.; Erra Sola, Montserrat; Aguilar Izquierdo, Nuria; Carrascal Riera, Marta; Taboada Martinez, Lorena; Navarro Romero, Eloisa; Vidal Juan, Bernat
Patent: EP2390252 A1, 2011 ;
Location in patent: Paragraph 0449; 0450 ;
EP 2390252 A1
反应条件
potassium permanganate
参考文献
Helvetica Chimica Acta, , vol. 36, p. 489,496
反应条件
diethyl ether; magnesium anschliessend mit CO2 behandeln;
参考文献
Journal of the Chemical Society, , p. 2455,246
反应条件
potassium permanganate
参考文献
Comment. phys. math., , vol. 19, # 1 p. 38
反应条件
sodium hydroxide; potassium chloride; potassium hexacyanoferrate(III) in methanol; water T=30°C; further temperature; activation energy; Thermodynamic dataKinetics;
参考文献
Journal of the Indian Chemical Society, , vol. 63, p. 1055 - 1059
反应条件
pyridine hydrochloride T=200°C; 0.5 h; Microwave irradiationIonic liquid;
参考文献
Cheng, Lili; Aw, Carlin; Ong, Siew Siang; Lu, Yixin
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 10 p. 2008 - 2010
反应条件
1.1: thionyl chloride / 31 h / 20 °C / Reflux
2.1: carbon disulfide / 0.5 h / Inert atmosphere; Cooling with ice
2.2: 19 h / 0 - 20 °C
3.1: ethyl mercaptan sodium salt / N,N-dimethyl-formamide / 16 h / 110 °C
View Scheme
参考文献
J-PHARMA CO., LTD.; WEMPE, Michael, F.; ENDOU, Hitoshi
Patent: WO2012/48058 A2, 2012 ;
WO 2012/048058 A2
