2,3-二氢-5-(2-羟基乙基)-6-甲基-2-硫氧代-1H-嘧啶-4-酮合成路线 （共 6 条）
反应条件
1: With ethanol; sodium 16 h; Heating / reflux; 2: With hydrogenchloride in water
参考文献
SOLVAY PHARMACEUTICALS B.V.
Patent: US2006/122206 A1, 2006 ;
Location in patent: Page/Page column 4 ;
US 20060122206 A1
参考文献
Ann.Rep.Tanabe pharm.Res.Chem.Abstr., , vol. 3, # 1 p. 4,7
Ann.Rep.Tanabe pharm.Res.Chem.Abstr., , p. 20183
Journal of the American Chemical Society, , vol. 67, p. 2197,2200
反应条件
sodium hydroxide; dihydrogen peroxide
参考文献
Kawanishi
Ann.Rep.Tanabe pharm.Res.Chem.Abstr., 1958 , vol. 3, # 1 p. 4,8
Ann.Rep.Tanabe pharm.Res.Chem.Abstr., 1958 , p. 20183
反应条件
hydrogen bromide
7 h; Heating; Yield given;
参考文献
Furukawa, Sunao; Takada, Mitsutaka; Castle, Raymond N.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 581 - 585
反应条件
1: 14 percent / 47percent HBr / 7 h / Heating
2: 90 percent / NaOH / H2O / 1 h / 100 °C
View Scheme
参考文献
Furukawa, Sunao; Takada, Mitsutaka; Castle, Raymond N.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 581 - 585
反应条件
hydrogen bromide
7 h; Heating; Yield given;
参考文献
Furukawa, Sunao; Takada, Mitsutaka; Castle, Raymond N.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 581 - 585
