2-甲氧基-2,4,6-环庚三烯-1-酮合成路线 （共 42 条）
反应条件
1: NaOEt 3: aq. KOH, EtOH 4: 200 °C View Scheme
参考文献
Nozoe,T. et al.
Bulletin of the Chemical Society of Japan, 1964 , vol. 37, # 11 p. 1644 - 1648
反应条件
N-bromosuccinmide 1 h; Heating;
参考文献
Takeshita, Hitoshi; Mori, Akira
Synthesis, 1986 , # 7 p. 578 - 579
反应条件
2,3,11,12-dicyclohexano-1,4,7,10,13,16-hexaoxacyclo-octadecane; potassium carbonate in acetonitrile
10 h; Heating;
参考文献
Nagahara; Nakano; Mimura; Nakamura; Uchida
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 12 p. 2491 - 2499
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in diethyl ether
T=20°C; Mitsunobu coupling;
参考文献
Houte, Henri; Valnot, Jean-Yves; Piettre, Serge R.
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9217 - 9220
反应条件
in methanol; diethyl ether
参考文献
Irvine, Nicholas M.; Majewski, Marek
Organic Preparations and Procedures International, 1995 , vol. 27, # 5 p. 592 - 595
反应条件
2,3,11,12-dicyclohexano-1,4,7,10,13,16-hexaoxacyclo-octadecane; potassium carbonate in acetonitrile
12 h; Heating;
参考文献
Joy, Abraham; Kaanumalle, Lakshmi S.; Ramamurthy
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 16 p. 3045 - 3053
反应条件
potassium carbonate in acetone
Methylation; 3 h; Heating;
参考文献
Chen, Arh-Hwang
Journal of the Chinese Chemical Society, 1999 , vol. 46, # 1 p. 35 - 39
反应条件
1: KMnO4; aq.-ethanolic KOH
View Scheme
参考文献
Doering; Knox
Journal of the American Chemical Society, 1951 , vol. 73, p. 828,838
反应条件
triethylamine in dichloromethane
25 h; Heating;
参考文献
Yagihara, Morio; Kitahara, Yoshio; Asao, Toyonobu
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 1 p. 236 - 238
反应条件
2,3,11,12-dicyclohexano-1,4,7,10,13,16-hexaoxacyclo-octadecane; potassium carbonate in acetonitrile
Alkylation; Heating;
参考文献
Koodanjeri, Smriti; Joy, Abraham; Ramamurthy
Tetrahedron, 2000 , vol. 56, # 36 p. 7003 - 7009
