1-甲氧基-1,3-环己二烯合成路线 （共 48 条）
反应条件
1: 95 percent / Et3N / CH2Cl2 / 24 h / Ambient temperature
2: 99 percent / AlCl3 / CH2Cl2 / 24 h / Ambient temperature
View Scheme
参考文献
Bloomer, James L.; Stagliano, Kenneth W.; Gazzillo, Joseph A.
Journal of Organic Chemistry, 1993 , vol. 58, # 27 p. 7906 - 7912
反应条件
1: 2) Ag2O / 1) benzene, reflux, 24 h, 2) DME
2: 54 percent / Heating
View Scheme
参考文献
Potts, Kevin T.; Bhattacharjee, Debkumar; Walsh, Eileen B.
Journal of Organic Chemistry, 1986 , vol. 51, # 11 p. 2011 - 2021
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Koyama, Junko; Morita, Izumi; Kobayashi, Norihiro; Osakai, Toshiyuki; Usuki, Yoshinosuke; Taniguchi, Makoto
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 4 p. 1079 - 1082
反应条件
in benzene
2 h; Heating;
参考文献
Hugo; Nicholson; Snijman
Synthetic Communications, 1994 , vol. 24, # 1 p. 23 - 28
反应条件
hydrogen; phenanthrene chrome tricarbonyle in cyclohexane
T=80°C; P=5320 Torr; 28 h; var. solvents, times; Product distribution;
参考文献
Maux, Paul Le; Simonneaux, Gerard
Journal of Organometallic Chemistry, 1982 , vol. 229, # 2 p. C24 - C26
反应条件
ethanol; ammonia; sodium
参考文献
Birch
Journal of the Chemical Society, 1947 , p. 1642,1647
参考文献
Krapcho; Bothner-By
Journal of the American Chemical Society, 1959 , vol. 81, p. 3658,3661, 3662, 3665
参考文献
Birch
Journal of the Chemical Society, 1947 , p. 1642,1647
反应条件
1: 79 percent / dichloromaleic anhydride, N-phenyl-β-naphthylamine / 26 h / 186 °C
2: 84 percent / p-TsOH / CH2Cl2 / 25 h / Ambient temperature
3: 97 percent / HBr, AcOH / 4 h / Heating
View Scheme
参考文献
Dimitriadis, Christian; Gill, Melvyn; Harte, Michael F.
Tetrahedron Asymmetry, 1997 , vol. 8, # 13 p. 2153 - 2158
反应条件
1: 83 percent / methanol / 1 h / Ambient temperature
2: 1.) NaH, 2.) Ag2O, MgSO4 / 1.) THF, 0 deg C, 30 min, 2.) THF, 1.5 h
3: 83 percent / p-toluenesulfonic acid / xylene / 1.25 h / Heating
View Scheme
参考文献
Tapia, Ricardo; Valderrama, Jaime A.; Quintanar, Carmina
Heterocycles, 1994 , vol. 38, # 8 p. 1797 - 1804
