反应条件
1.1: tetrahydrofuran / 0.17 h / |Cooling with ice
2.1: sec.-butyllithium; N,N,N',N,-tetramethylethylenediamine / tetrahydrofuran / 0.5 h / -78 °C
2.2: 4.25 h / -78 - 20 °C
View Scheme
参考文献
Dittmann, Marc; Graupner, Franziska F.; Maerz, Benjamin; Oesterling, Sven; Devivie-Riedle, Regina; Zinth, Wolfgang; Engelhard, Martin; Luettke, Wolfgang
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 591 - 594
Angew. Chem., 2013 , vol. 126, # 2 p. 602 - 605,4