1: 4-dimethylaminopyridine, pyridine / benzene / 4 h / Ambient temperature 2: 56 percent / diethyl ether; benzene / 6 h / Ambient temperature 3: 91 percent / aq. KOH / ethanol / 0.5 h / Heating View Scheme
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1: tert.-butyl lithium With copper(I) bromide dimethylsulfide complex in tetrahydrofuran; pentane T=-78°C; Inert atmosphere; 2: 2-methoxy-benzoyl chloride in tetrahydrofuran; pentane T=-78°C; Inert atmosphere;
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Diaz-Valenzuela, M. Belen; Phillips, Scott D.; France, Marcia B.; Gunn, Mary E.; Clarke, Matthew L.
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1: sodium hydroxide / water / 2 h / 30 °C 2: rat cecal content / 37 °C / pH 6.8 / aq. phosphate buffer View Scheme
参考文献
Kong, Hyesik; Kim, Hyunjeong; Do, Heejeong; Lee, Yonghyun; Hong, Sungchae; Yoon, Jeong-Hyun; Jung, Yunjin; Kim, Young Mi
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