3-环戊烯-1,1-二甲酸二乙酯合成路线 （共 19 条）
反应条件
pig liver esterase; water; sodium chloride
T=20°C; 25 h; Enzymatic reaction;
参考文献
Tenbrink, Katharina; Sessler, Miriam; Schatz, Juergen; Groeger, Harald
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 13 p. 2363 - 2367
反应条件
pig liver esterase; water; sodium chloride
T=20°C; 12 h; Enzymatic reaction;
参考文献
Tenbrink, Katharina; Sessler, Miriam; Schatz, Juergen; Groeger, Harald
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 13 p. 2363 - 2367
反应条件
pig liver esterase; water; sodium chloride
T=20°C; 42 h; Enzymatic reaction;
参考文献
Tenbrink, Katharina; Sessler, Miriam; Schatz, Juergen; Groeger, Harald
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 13 p. 2363 - 2367
反应条件
1: 65.7 percent / KOH / ethanol / 20 h / Ambient temperature
2: 89.4 percent / SOCl2 / toluene / 2 h / Heating
View Scheme
参考文献
Paulsen, Hans; Maass, Uwe
Chemische Berichte, 1981 , vol. 114, # 1 p. 346 - 358
反应条件
1: 65.7 percent / KOH / ethanol / 20 h / Ambient temperature
2: 89.4 percent / SOCl2 / toluene / 2 h / Heating
3: NaN3 / H2O; acetone / 0.5 h / 0 °C
4: benzene / 0.5 h / Heating
5: 73 percent / LiAlH4 / diethyl ether / 20 h / Ambient temperature
View Scheme
参考文献
Paulsen, Hans; Maass, Uwe
Chemische Berichte, 1981 , vol. 114, # 1 p. 346 - 358
反应条件
potassium hydroxide in ethanol
T=70°C;
参考文献
Kotha, Sambasivarao; Deb, Ashoke Chandra
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2008 , vol. 47, # 7 p. 1120 - 1134
反应条件
1: KOH / H2O; ethanol / 6 h / Heating
2: 180 °C
3: 79 percent / LiAlH4 / diethyl ether
4: 79 percent / SOCl2, pyridine / 1 h / Heating
5: 1.) Mg / 1.) ether, 2.) ether, 10 h
View Scheme
参考文献
Hosomi; Mikami; Sakurai
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2784 - 2794
反应条件
C41H61ClN3O2PRu
T=70°C; 71 h; Inert atmosphereSchlenk technique;
参考文献
Wdowik, Tomasz; Samojlowicz, Cezary; Jawiczuk, Magdalena; Malinska, Maura; Wozniak, Krzysztof; Grela, Karol
Chemical Communications, 2013 , vol. 49, # 7 p. 674 - 676
反应条件
1: 84 percent / LiAlH4 / diethyl ether / 2 h / 20 °C
2: 98 percent / p-TsOH / dimethylformamide / 4 h / 20 °C
View Scheme
参考文献
Kang, Ji-Hye; Chung, Hye-Eun; Kim, Su Yeon; Kim, Yerim; Lee, Jeewoo; Lewin, Nancy E.; Pearce, Larry V.; Blumberg, Peter M.; Marquez, Victor E.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 12 p. 2529 - 2539
