1-(3-乙酰基-2,6-二羟基苯基)乙酮合成路线 (共 29 条)
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Rosenmund; Buchwald; Deligiannis
Archiv der Pharmazie (Weinheim, Germany), 1933 , vol. 271, p. 342,348
反应条件
sodium acetate 2 h; Heating;
参考文献
Essawy, S. A.; El-Kady, M. Y.; Donia, S. G.; El-Shenawy, A. I.
Egyptian Journal of Chemistry, 1994 , vol. 37, # 4 p. 381 - 390
反应条件
hydrogenchloride; zinc(II) chloride in water
T=140°C; 24 h;
参考文献
Vijaya Bhaskar Reddy; Shen, Yuh-Chiang; Ohkoshi, Emika; Bastow, Kenneth F.; Qian, Keduo; Lee, Kuo-Hsiung; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 47, # 1 p. 97 - 103
反应条件
N,N-dimethyl-formamide; zinc
T=54°C; Fries rearrangement; 2.25 h; microwave irradiation;
参考文献
Paul, Satya; Gupta, Monika
Synthesis, 2004 , # 11 p. 1789 - 1792
反应条件
zinc(II) chloride
T=145 - 150°C; 0.25 h;
参考文献
Anjaneyulu, A. S. R.; Mallavadhani, U. V.; Venkateswarlu, Y.; Prasad, A. V. Rama
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 823 - 826
反应条件
aluminium trichloride
T=120°C; 2 h;
参考文献
Kotali, Antigoni
Tetrahedron Letters, 1994 , vol. 35, # 36 p. 6753 - 6754
反应条件
dichloro bis(acetonitrile) palladium(II) in 1,4-dioxane
0.75 h; Heating;
参考文献
Anjaneyulu, Ammanamanchi S. R.; Isaa, Balagopala M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 9 p. 2089 - 2094
反应条件
boron trifluoride; acetic acid
T=140°C; Behandeln des Reaktionsprodukts mit wss.Natriumacetat;
参考文献
Oelschlaeger
Archiv der Pharmazie (Weinheim, Germany), 1955 , vol. 288, p. 102,107,108
参考文献
Israelstam
Journal of the South African Chemical Institute, 1944 , vol. 27, p. 15,17
反应条件
hydrogenchloride; acetic acid
T=160 - 170°C;
参考文献
Desai; Radha
Proceedings - Indian Academy of Sciences, Section A, 1940 , vol. <A> 12, p. 46,48