11-哌嗪基二苯并[b,f][1,4]氧氮杂卓合成路线 （共 6 条）
参考文献
Allelix Biopharmaceuticals Inc.
Patent: US5834459 A1, 1998 ;
US 5834459 A
参考文献
Wagh; Patil; Jain; Harak
Heterocyclic Communications, 2007 , vol. 13, # 2-3 p. 165 - 172
反应条件
1: 82 percent / H2 / Raney nickel W-2 / methanol / 3620.13 Torr
2: 3.4 g / H2SO4 / dimethylformamide / 15 h / Heating
3: 40 percent / POCl3; N,N-dimethylaniline / Heating
4: 88 percent / xylene / Heating
View Scheme
参考文献
Wagh; Patil; Jain; Harak
Heterocyclic Communications, 2007 , vol. 13, # 2-3 p. 165 - 172
反应条件
1: 93 percent / K2CO3 / 10 h / Heating
2: 82 percent / H2 / Raney nickel W-2 / methanol / 3620.13 Torr
3: 3.4 g / H2SO4 / dimethylformamide / 15 h / Heating
4: 40 percent / POCl3; N,N-dimethylaniline / Heating
5: 88 percent / xylene / Heating
View Scheme
参考文献
Wagh; Patil; Jain; Harak
Heterocyclic Communications, 2007 , vol. 13, # 2-3 p. 165 - 172
反应条件
1: 40 percent / POCl3; N,N-dimethylaniline / Heating
2: 88 percent / xylene / Heating
View Scheme
参考文献
Wagh; Patil; Jain; Harak
Heterocyclic Communications, 2007 , vol. 13, # 2-3 p. 165 - 172
反应条件
1: 3.4 g / H2SO4 / dimethylformamide / 15 h / Heating
2: 40 percent / POCl3; N,N-dimethylaniline / Heating
3: 88 percent / xylene / Heating
View Scheme
参考文献
Wagh; Patil; Jain; Harak
Heterocyclic Communications, 2007 , vol. 13, # 2-3 p. 165 - 172
