2-苄基异喹啉-1,3,4-三酮合成路线 （共 10 条）
反应条件
1: Phthalonimide With sodium hydride in N,N-dimethyl-formamide
T=-15°C; 0.333333 h;
2: benzyl chloride in N,N-dimethyl-formamide
T=20°C; 2 h;
参考文献
Chen, Yi-Hua; Zhang, Ya-Hui; Zhang, Hua-Jie; Liu, Da-Zhi; Gu, Min; Li, Jing-Ya; Wu, Fang; Zhu, Xing-Zu; Li, Jia; Nan, Fa-Jun
Journal of Medicinal Chemistry, 2006 , vol. 49, # 5 p. 1613 - 1623
反应条件
ruthenium(IV) oxide; sodium periodate in ethyl acetate
3.5 h; Ambient temperature;
参考文献
Yoshifuji; Arakawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 12 p. 3380 - 3381
反应条件
ruthenium(IV) oxide; sodium periodate in ethyl acetate
4 h; Ambient temperature;
参考文献
Yoshifuji; Arakawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 12 p. 3380 - 3381
反应条件
oxygen; thiamine diphosphate in pyridine; benzene
Oxidation; 12 h; Irradiation;
参考文献
Ling, Ke-Qing; Ye, Jia-Hai; Chen, Xian-Yang; Ma, De-Jian; Xu, Jian-Hua
Tetrahedron, 1999 , vol. 55, # 30 p. 9185 - 9204
反应条件
1: benzene / Heating
2: KOH-K3Fe(CN)6 / H2O; benzene / Ambient temperature
3: hydrogen / Raney nickel W-2 / ethanol / 2584 Torr / Ambient temperature
4: 81 percent / RuO2*xH2O, 10percent aqueous NaIO4 / ethyl acetate / 4 h / Ambient temperature
View Scheme
参考文献
Yoshifuji; Arakawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 12 p. 3380 - 3381
反应条件
1: hydrogen / Raney nickel W-2 / ethanol / 2584 Torr / Ambient temperature
2: 81 percent / RuO2*xH2O, 10percent aqueous NaIO4 / ethyl acetate / 4 h / Ambient temperature
View Scheme
参考文献
Yoshifuji; Arakawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 12 p. 3380 - 3381
反应条件
1: KOH-K3Fe(CN)6 / H2O; benzene / Ambient temperature
2: hydrogen / Raney nickel W-2 / ethanol / 2584 Torr / Ambient temperature
3: 81 percent / RuO2*xH2O, 10percent aqueous NaIO4 / ethyl acetate / 4 h / Ambient temperature
View Scheme
参考文献
Yoshifuji; Arakawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 12 p. 3380 - 3381
反应条件
1: benzene / Heating
2: KOH-K3Fe(CN)6 / H2O; benzene / Ambient temperature
3: hydrogen / Raney nickel W-2 / ethanol / 2584 Torr / Ambient temperature
4: 81 percent / RuO2*xH2O, 10percent aqueous NaIO4 / ethyl acetate / 4 h / Ambient temperature
View Scheme
参考文献
Yoshifuji; Arakawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 12 p. 3380 - 3381
反应条件
1: 80 percent / 180 °C
2: 78 percent / O2; TPP / benzene; pyridine / 12 h / Irradiation
View Scheme
参考文献
Ling, Ke-Qing; Ye, Jia-Hai; Chen, Xian-Yang; Ma, De-Jian; Xu, Jian-Hua
Tetrahedron, 1999 , vol. 55, # 30 p. 9185 - 9204
反应条件
1: 80 percent / 180 °C
2: 78 percent / O2; TPP / benzene; pyridine / 12 h / Irradiation
View Scheme
参考文献
Ling, Ke-Qing; Ye, Jia-Hai; Chen, Xian-Yang; Ma, De-Jian; Xu, Jian-Hua
Tetrahedron, 1999 , vol. 55, # 30 p. 9185 - 9204
