3-(3-甲基苯基)苯甲醛合成路线 (共 2 条)
反应条件
1: 1-chloro-3-methylbenzene With tetrahydroxydiboron; ethanol; XPhos-Pd-G2; potassium acetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water T=80°C; Miyaura Borylation Reaction; 15 h; Inert atmosphere; 2: 3-chloro-benzaldehyde With potassium carbonate in water T=80°C; Suzuki Coupling; 15 h; Inert atmosphere;
参考文献
Molander, Gary A.; Trice, Sarah L. J.; Kennedy, Steven M.
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8678 - 8688