2-甲基-6-苯基吡嗪-3(2h)-酮合成路线 (共 7 条)
反应条件
pyridine; oxygen; copper diacetate; sodium carbonate in toluene T=20 - 100°C; 12 h; chemoselective reaction;
参考文献
Liang, Lei; Yang, Guanyu; Xu, Fengrong; Niu, Yan; Sun, Qi; Xu, Ping
European Journal of Organic Chemistry, 2013 , # 27 p. 6130 - 6136
反应条件
in N,N-dimethyl-formamide Heating;
参考文献
Sotelo, Eddy; Ravina, Enrique
Synthetic Communications, 2002 , vol. 32, # 11 p. 1675 - 1680
反应条件
1: 72 percent / acetic acid / Heating 2: 81 percent / Br2 / acetic acid / 1 h / 80 °C View Scheme
参考文献
Volynets, N. F.; Smartseva, I. V.; Khramova, I. V.; Pavlova, L. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , p. 1604 - 1608
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 8 p. 1760 - 1764
参考文献
Duffin; Kendall
Journal of the Chemical Society, 1959 , p. 3789,3794
反应条件
in N,N-dimethyl-formamide T=5°C; 24 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 28, # 2 p. 417 - 423
反应条件
acetic acid; zinc 3 h; Heating; Yield given;
参考文献
Brown, George R.; Foubister, Alan J.; Wright, Brian
Journal of the Chemical Society, Chemical Communications, 1984 , # 20 p. 1373 - 1374
反应条件
acetic acid; zinc
6 h; Heating; Yield given. Yields of byproduct given;
参考文献
Brown, George R.; Foubister, Alan J.; Wright, Brian
Journal of the Chemical Society, Chemical Communications, 1984 , # 20 p. 1373 - 1374