N,N′,N′′-三叔丁氧羰基胍合成路线 (共 3 条)
反应条件
potassium hydroxide; sodium carbonate 1.) DMSO, 5 min; other reagent: sodium hydroxide, 2.) DMSO, 40 deg C, 60 h; Yield givenMultistep reaction;
参考文献
Cesco-Cancian, Sergio; Chen, Hongfeng; Grimm, Jeffrey S.; Mani, Neelakandha S.; Mapes, Christopher M.; Palmer, David C.; Pippel, Daniel J.; Sorgi, Kirk L.; Xiao, Tong
Patent: US2010/4450 A1, 2010 ;
Location in patent: Page/Page column 22 ;
反应条件
sodium hydroxide in 1,4-dioxane T=0 - 20°C; 26 h;
参考文献
Castillo-Melendez, Joel A.; Golding, Bernard T.
Synthesis, 2004 , # 10 p. 1655 - 1663
反应条件
sodium hydroxide 1.) dioxane, water, 2.) dioxane, water, room temperature; Yield givenMultistep reaction;
参考文献
Feichtinger, Konrad; Sings, Heather L.; Baker, Tracy J.; Matthews, Kenneth; Goodman, Murray
Journal of Organic Chemistry, 1998 , vol. 63, # 23 p. 8432 - 8439