6-苯基-3(2H)-哒嗪酮合成路线 (共 69 条)
反应条件
hydrazine hydrate in tert-butyl alcohol Reflux;
参考文献
Journal of Organic Chemistry, , vol. 77, # 21 p. 9865 - 9870,6
反应条件
1: 94 percent / butan-1-ol / 1.) 95 deg C, 2 min; 2.) -20 deg C 2: CH3CO2H / butan-1-ol / 0.9 h / 140 °C / various reagents, temperatures, and times View Scheme
参考文献
Bulletin de la Societe Chimique de France, , # 5 p. 865 - 870
反应条件
hydrogen iodide in ethanol 4 h; Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 20, # 12 p. 1084 - 1086
反应条件
1: 79 percent / sodamide / 48 h / Heating 2: hydroiodic acid / ethanol / 4 h / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 20, # 12 p. 1084 - 1086
反应条件
ammonia; hydrazine hydrate in water pH=8; 2 h; Reflux;
参考文献
Arzneimittel-Forschung/Drug Research, , vol. 59, # 7 p. 357 - 363
反应条件
1: phosphorus oxychloride / 4 h / 85 - 95 °C 2: hydrazine hydrate / butan-1-ol / 6 h / 100 °C View Scheme
参考文献
Wermuth, Camille-Georges; Bourguignon, Jean-Jacques; Schlewer, Gilbert; Gies, Jean-Pierre; Schoenfelder, Angele; et al.
Journal of Medicinal Chemistry, 1987 , vol. 30, # 2 p. 239 - 249
反应条件
in N,N-dimethyl-formamide Heating;
参考文献
Sotelo, Eddy; Ravina, Enrique
Synthetic Communications, 2002 , vol. 32, # 11 p. 1675 - 1680
参考文献
Duffin; Kendall
Journal of the Chemical Society, 1959 , p. 3789,3794
反应条件
in tetrahydrofuran; toluene T=20°C; Heating / reflux;
参考文献
Watterson, D. Martin; Van Eldik, Linda; Hu, Wenhui
Patent: US2009/325973 A1, 2009 ;
Location in patent: Page/Page column 29 ;
参考文献
Yamada, Toshihiro; Shimamura, Hiroshi; Tsukamoto, Yoshitsugu; Yamaguchi, Azuma; Ohki, Masahiko
Journal of Medicinal Chemistry, 1983 , vol. 26, # 8 p. 1144 - 1149