(E)-4-十一烯-1-醇合成路线 （共 4 条）
参考文献
Paul; Tchelitcheff
Bulletin de la Societe Chimique de France, 1948 , p. 1200
反应条件
1: PBr3 / toluene 2: (i) Na, nBuOH, (ii) aq. KOH, (iii) (heating) 3: LiAlH4 4: PBr3 / toluene 5: dimethylsulfoxide 6: H2, EtOH / Pd-CaCO3, Pd-BaSO4 / hexane View Scheme
参考文献
Voaden,D.J.; Jacobson,M.
Journal of Medicinal Chemistry, 1972 , vol. 15, p. 619 - 623
反应条件
pyridinium chlorochromate in dichloromethane
2 h;
参考文献
Bestmann; Koschatzky; Schaetzke; et al.
1981 , vol. No. 9, p. 1705 - 1720
反应条件
1.1: Et3N / CH2Cl2 / 0.33 h / -50 - -20 °C
2.1: 0.66 g / NaN3 / dimethylsulfoxide / 16 h
3.1: mercuric perchlorate trihydrate / tetrahydrofuran / 0.75 h / 20 °C
3.2: 58 percent / sodium borohydride; sodium hydroxide / H2O; tetrahydrofuran / 2 h
View Scheme
参考文献
Pearson; Hutta; Fang
Journal of Organic Chemistry, 2000 , vol. 65, # 24 p. 8326 - 8332
