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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2′-氟脱氧腺苷
合成路线
（共 12 条）
259528-01-3
→
反应条件
21679-12-9
2′-氟脱氧腺苷
反应条件
tetraethyl ammonium fluoride in acetonitrile T=20°C; Substitution; 0.5 h;
参考文献
Hassan, Abdalla E. A.; Shortnacy-Fowler, Anita T.; Montgomery, John A.; Secrist III, John A.
Nucleosides, Nucleotides and Nucleic Acids, 2000 , vol. 19, # 3 p. 559 - 565
675598-20-6
→
反应条件
21679-12-9
2′-氟脱氧腺苷
反应条件
tetraethyl ammonium fluoride in acetone T=20°C;
参考文献
Ye, Song; Rezende, Martha M.; Deng, Wei-Ping; Kirk, Kenneth L.
Nucleosides, Nucleotides and Nucleic Acids, 2003 , vol. 22, # 10 p. 1899 - 1905
951-78-0
2'-脱氧尿苷
+
700-49-2
2-氟-6-氨基嘌呤
→
反应条件
21679-12-9
2′-氟脱氧腺苷
反应条件
aeromonas hydrophila CECT 4226 T=45°C; pH=7; 1 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Nbile, Matas; Terreni, Marco; Lewkowicz, Elizabeth; Iribarren, Adolfo M.
Biocatalysis and Biotransformation, 2010 , vol. 28, # 5-6 p. 395 - 402
146-78-1
2-氟腺苷
→
反应条件
21679-12-9
2′-氟脱氧腺苷
反应条件
1: 52 percent / imidazole / dimethylformamide / 4 h / 20 °C 2: 81 percent / DMAP / 1,2-dichloro-ethane / 2 h / Heating 3: 96 percent / tert-butyl peroxide; TTMSS / dioxane; toluene / 0.25 h / 80 °C 4: 98 percent / Et4NF*xH2O / acetonitrile / 0.5 h / 20 °C View Scheme
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 19, # 3 p. 559 - 565
111556-91-3
→
反应条件
21679-12-9
2′-氟脱氧腺苷
反应条件
1: 81 percent / DMAP / 1,2-dichloro-ethane / 2 h / Heating 2: 96 percent / tert-butyl peroxide; TTMSS / dioxane; toluene / 0.25 h / 80 °C 3: 98 percent / Et4NF*xH2O / acetonitrile / 0.5 h / 20 °C View Scheme
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 19, # 3 p. 559 - 565
452-51-7
→
反应条件
21679-12-9
2′-氟脱氧腺苷
反应条件
1.1: 94 percent / Dowex 50wx-100 ion-exchange resin / 17 h / 20 °C 2.1: 78 percent / DMAP; Et3N / CH2Cl2; dimethylformamide / 0 - 20 °C 3.1: zinc iodide; tetrabutylammnoum iodide / CH2Cl2 / 1 h / -15 °C 4.1: ammonium sulfate; hexamethyldisilazane / Heating 4.2: 32 percent / 4 Angstroem molecular sieves; NBS / toluene / 0 - 20 °C 5.1: 87 percent / tetraethylammonium fluoride hydrate / acetone / 20 °C View Scheme
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 22, # 10 p. 1899 - 1905
700-49-2
2-氟-6-氨基嘌呤
→
反应条件
21679-12-9
2′-氟脱氧腺苷
反应条件
1.1: ammonium sulfate; hexamethyldisilazane / Heating 1.2: 32 percent / 4 Angstroem molecular sieves; NBS / toluene / 0 - 20 °C 2.1: 87 percent / tetraethylammonium fluoride hydrate / acetone / 20 °C View Scheme
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 22, # 10 p. 1899 - 1905
675598-22-8
→
反应条件
21679-12-9
2′-氟脱氧腺苷
反应条件
1.1: zinc iodide; tetrabutylammnoum iodide / CH2Cl2 / 1 h / -15 °C 2.1: ammonium sulfate; hexamethyldisilazane / Heating 2.2: 32 percent / 4 Angstroem molecular sieves; NBS / toluene / 0 - 20 °C 3.1: 87 percent / tetraethylammonium fluoride hydrate / acetone / 20 °C View Scheme
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 22, # 10 p. 1899 - 1905
174289-74-8
→
反应条件
21679-12-9
2′-氟脱氧腺苷
反应条件
1.1: ammonium sulfate; hexamethyldisilazane / Heating 1.2: 32 percent / 4 Angstroem molecular sieves; NBS / toluene / 0 - 20 °C 2.1: 87 percent / tetraethylammonium fluoride hydrate / acetone / 20 °C View Scheme
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 22, # 10 p. 1899 - 1905
268217-17-0
→
反应条件
21679-12-9
2′-氟脱氧腺苷
反应条件
1: 96 percent / tert-butyl peroxide; TTMSS / dioxane; toluene / 0.25 h / 80 °C 2: 98 percent / Et4NF*xH2O / acetonitrile / 0.5 h / 20 °C View Scheme
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 19, # 3 p. 559 - 565
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