(+)-(2R,3R,11R,12R)-1,4,7,10,13,16-hexaoxacyclooctadecane-2,3,11,12-tetracarboxylic acid in various solvent(s)
T=25°C; pH=2.5; Electrochemical reaction;
1: trans-cyclo(Val-D-Phe) With hydrogenchloride
72 h; Heating;
2: methanol With thionyl chloride
16 h; Heating; Further stages.;
参考文献
Davies, Stephen G.; Christopher Garner; Ouzman, Jaqueline V. A.; Roberts, Paul M.; Smith, Andrew D.; Snow, Emma J.; Thomson, James E.; Tamayo, Juan A.; Vickers, Richard J.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 13 p. 2138 - 2147