反应条件
1: 1.) lithium hexamethyldisilazide / 1.) THF, 0 deg C, 2 h, 2.) THF, -78 deg C, 3 h
2: 1.) 57percent HI, 2.) SOCl2 / 1.) reflux, 1 h, 2.) from -10 deg C to RT, 14 h
View Scheme
参考文献
Orena, Mario; Porzi, Gianni; Sandri, Sergio
Journal of Chemical Research, Miniprint, 1993 , # 8 p. 2125 - 2152
