1-烯丙基-1.2-二甲酰基肼合成路线 （共 3 条）
反应条件
T=80°C; Formylation; 15 h;
参考文献
Kumagai, Toshio; Tamai, Satoshi; Abe, Takao; Matsunaga, Hiroshi; Hayashi, Kazuhiko; Kishi, Ikuo; Shiro, Motoo; Nagao, Yoshimitsu
Journal of Organic Chemistry, 1998 , vol. 63, # 23 p. 8145 - 8149
反应条件
1: 95 percent / LiBr*H2O; Br2 / CH2Cl2; methanol / 0.17 h / 0 °C 2: 74 percent / K2CO3 / ethyl acetate / 6 h / 40 °C 3: 95 percent / ethyl acetate / 6 h / 40 °C View Scheme
参考文献
Kumagai, Toshio; Tamai, Satoshi; Abe, Takao; Matsunaga, Hiroshi; Hayashi, Kazuhiko; Kishi, Ikuo; Shiro, Motoo; Nagao, Yoshimitsu
Journal of Organic Chemistry, 1998 , vol. 63, # 23 p. 8145 - 8149
反应条件
1: 95 percent / LiBr*H2O; Br2 / CH2Cl2; methanol / 0.17 h / 0 °C 2: 74 percent / K2CO3 / ethyl acetate / 6 h / 40 °C View Scheme
参考文献
Kumagai, Toshio; Tamai, Satoshi; Abe, Takao; Matsunaga, Hiroshi; Hayashi, Kazuhiko; Kishi, Ikuo; Shiro, Motoo; Nagao, Yoshimitsu
Journal of Organic Chemistry, 1998 , vol. 63, # 23 p. 8145 - 8149
