反式-α-氰基肉桂酸乙酯合成路线 (共 30 条)
反应条件
methyl(diphenyl)-phosphine in toluene T=110°C; 5 h; Inert atmosphere;
参考文献
Siby, Acetou; Loreau, Olivier; Taran, Frederic
Synthesis, 2009 , # 14 art. no. Z05209SS, p. 2365 - 2370
反应条件
tri-n-butyl-arsine T=80°C; 5 h;
参考文献
Shen, Yanchang; Yang, Baozhen
Synthetic Communications, 1989 , vol. 19, # 17 p. 3069 - 3076
反应条件
dimethyl sulfoxide T=20°C; Knoevenagel condensation; 2.5 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Chiba, Ryoichi; Oriyama, Takeshi
Chemistry Letters, 2008 , vol. 37, # 12 p. 1218 - 1219
反应条件
Ru(PPh3)3(CO)H2; piperidinium acetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene 24 h; Heating;
参考文献
Tetrahedron Letters, , vol. 47, # 38 p. 6787 - 6789
反应条件
morpholine in water T=20°C; Knoevenagel condensation; 2 h; optical yield given as percent de;
参考文献
Synthetic Communications, , vol. 41, # 1 p. 52 - 57
反应条件
acetate-intercalated NiZn mixed basic salt in water T=50°C; Knoevenagel Condensation; 1 h; Inert atmosphere;
参考文献
Hara, Takayoshi; Kurihara, Jun; Ichikuni, Nobuyuki; Shimazu, Shogo
Chemistry Letters, 2010 , vol. 39, # 3 p. 304 - 305
反应条件
1: oxygen / water / 1.5 h / 79.84 °C / 750.08 Torr 2: air; Pd1–Au1 bimetal catalysts supported on basic layered double hydroxide / 1 h / 353 °C View Scheme
参考文献
Catalysis Communications, , vol. 47, p. 49 - 53
反应条件
H-beta zeolite T=80°C; Knoevenagel condensation; 22 h; Inert atmosphereNeat (no solvent);
参考文献
Journal of Catalysis, , vol. 285, # 1 p. 10 - 18
参考文献
Justus Liebigs Annalen der Chemie, , vol. 578, p. 101,112
反应条件
T=80°C; 5 h; Inert atmosphereNeat (no solvent);
参考文献
Journal of Catalysis, , vol. 285, # 1 p. 10 - 18