反式-α-氰基肉桂酸乙酯合成路线 （共 30 条）
反应条件
water; sodium hydrogencarbonate; lithium chloride in dimethyl sulfoxide T=165°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Babler, James H.; Spina, Kenneth P.
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3835 - 3838
反应条件
1: 77 percent / 0.4M K2CO3 / methanol; H2O / 0.5 h / Heating 2: 4LiCl-4H2O-2NaHCO3 / dimethylsulfoxide / 3 h / 165 °C / also with NaCl; reagent conc., temp., reaction time varied; other substrates: CH3 and C2H5 esters of this acid; stereochemistry investigated View Scheme
参考文献
Babler, James H.; Spina, Kenneth P.
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3835 - 3838
反应条件
Re(NCCHCO2Et)lt;NC(EtO2C)C=CHPhgt;(PMe2Ph)4 in dimethyl sulfoxide 99 h; Ambient temperaturecatalytic metathesis of substituted olefins promoted by rhenium(I) enolate complexes, var. rhenium(I) enolate complex; Product distribution;
参考文献
Hirano, Masafumi; Hirai, Miwa; Ito, Yuji; Fukuoka, Atsushi; Komiya, Sanshiro
Chemistry Letters, 1994 , # 1 p. 165 - 166
反应条件
N-benzyl-N,N,N-trimethyl-ammonium chloride in acetonitrile 0.25 h;
参考文献
Beletskii; Kuznetsov
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 8 p. 1229 - 1240
反应条件
in ethanol 4 h; Heating;
参考文献
Babler, James H.; Spina, Kenneth P.
Tetrahedron Letters, 1984 , vol. 25, # 16 p. 1659 - 1660
反应条件
water; sodium hydrogencarbonate; lithium chloride in dimethyl sulfoxide
T=165°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Babler, James H.; Spina, Kenneth P.
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3835 - 3838
反应条件
1: 77 percent / 0.4M K2CO3 / methanol; H2O / 0.5 h / Heating
2: 4LiCl-4H2O-2NaHCO3 / dimethylsulfoxide / 3 h / 165 °C / also with NaCl; reagent conc., temp., reaction time varied; other substrates: CH3 and C2H5 esters of this acid; stereochemistry investigated
View Scheme
参考文献
Babler, James H.; Spina, Kenneth P.
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3835 - 3838
反应条件
aluminum tri-bromide
0.28 h; Ambient temperature;
参考文献
Fuji, Kaoru; Kawabata, Takeo; Node, Manabu; Fujita, Eiich
Tetrahedron Letters, 1981 , vol. 22, p. 875 - 878
反应条件
formic acid; triethylamine; N-(2-amino-ethyl)-4-methyl-benzenesulphonamide; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2 in dichloromethane
T=30°C; 2 h;
参考文献
Xue, Dong; Chen, Ying-Chun; Cui, Xin; Wang, Qi-Wei; Zhu, Jin; Deng, Jin-Gen
Journal of Organic Chemistry, 2005 , vol. 70, # 9 p. 3584 - 3591
参考文献
Carrie
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1956 , vol. 243, p. 1213
