3,4-二甲氧基苯甲醛肟合成路线 （共 21 条）
反应条件
1: (hydroxy(tosyloxy)iodo)benzene / dimethyl sulfoxide / 1.5 h / 20 - 80 °C 2: sodium hydroxide / dimethyl sulfoxide / 1.5 h / 80 °C View Scheme
参考文献
Arkivoc, , vol. 2011, # 2 p. 209 - 216
反应条件
chloramine-T in ethanol T=20°C; Dehydrogenation; oxidation; 0.0333333 h;
参考文献
Cha, Mi Young; Choi, Byung Chul; Kang, Kyung Ho; Pae, Ae Nim; Choi, Kung Il; Cho, Yong Seo; Koh, Hun Yeong; Lee, Hee-Yon; Jung, Daeyoung; Kong, Jae Yang
Bioorganic & Medicinal Chemistry Letters, 2002 , vol. 12, # 10 p. 1327 - 1330
反应条件
[η5-pentamethylcyclopentadienyl*Ir(H2O)3][OTf ]2 in water T=110°C; 12 h; Schlenk technique;
参考文献
Sun, Chunlou; Qu, Panpan; Li, Feng
Catalysis Science and Technology, 2014 , vol. 4, # 4 p. 988 - 996
反应条件
copper(II)-modified 4Å molecular sieve in acetonitrile T=80°C; 8 h;
参考文献
Kiss, Arpad; Hell, Zoltan
Synthetic Communications, 2013 , vol. 43, # 13 p. 1778 - 1786
反应条件
monomeric metaboric acid T=151 - 155°C; Beckmann rearrangement; 30 h;
参考文献
Chandrasekhar, Sosale; Gopalaiah, Kovuru
Tetrahedron Letters, 2002 , vol. 43, # 13 p. 2455 - 2457
反应条件
(hydroxy(tosyloxy)iodo)benzene in dimethyl sulfoxide T=20 - 80°C; 1.5 h;
参考文献
Ghosh, Harisadhan; Baneerjee, Arghya; Rout, Saroj Kumar; Patel, Bhisma K.
Arkivoc, 2011 , vol. 2011, # 2 p. 209 - 216
反应条件
silica gel 0.0166667 h; microwave irradiation;
参考文献
Dewan, Sharwan K.; Singh, Ravinder
Synthetic Communications, 2003 , vol. 33, # 17 p. 3085 - 3088
反应条件
copper(II)-modified 4Å molecular sieve in acetonitrile T=80°C; 8 h;
参考文献
Synthetic Communications, , vol. 43, # 13 p. 1778 - 1786
反应条件
monomeric metaboric acid T=151 - 155°C; Beckmann rearrangement; 30 h;
参考文献
Chandrasekhar, Sosale; Gopalaiah, Kovuru
Tetrahedron Letters, 2002 , vol. 43, # 13 p. 2455 - 2457
反应条件
0.5 h; microwave irradiation; Title compound not separated from byproducts;
参考文献
Kusurkar; Kannadkar
Synthetic Communications, 2001 , vol. 31, # 15 p. 2235 - 2239
