2-羟基-3-甲氧基苯甲醛 肟合成路线 （共 11 条）
反应条件
hydroxylamine hydrochloride; sodium acetate in water T=45 - 80°C;
参考文献
Hewitt, Ian J.; Lan, Yanhua; Anson, Christopher E.; Luzon, Javier; Sessoli, Roberta; Powell, Annie K.
Chemical Communications, 2009 , # 44 p. 6765 - 6767
反应条件
1: 80 percent / diethyl ether / 1.) -70 grad C, 2 h, 2.) 0 grad C, 4 h, 3.) room temperature, 3 days 2: aq. NaOH View Scheme
参考文献
Bonsignore, Leonardo; Loy, Guiseppe; Secci, Mario
Tetrahedron Letters, 1983 , vol. 24, # 45 p. 5013 - 5016
反应条件
thionyl chloride in diethyl ether Heating;
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2973 - 2978
反应条件
iron(III) chloride in benzene Heating;
参考文献
Hangarge; Mane; Chavan; Shingare
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 6 p. 1302 - 1304
反应条件
1: sodium acetate
2: diethyl ether / anschliessend Behandeln mit wss. HCl
View Scheme
参考文献
Richtzenhain
Chemische Berichte, 1944 , vol. 77/79, p. 1,5
反应条件
hydrogen; platinum(IV) oxide in acetic acid
P=3000.3 Torr; Product distribution / selectivity;
参考文献
Exposito, Miriam Royo; Clauzel, Luc Marti; Martin, Anna Abella; Vicente, Silvia Garcia; Yinbert, Xavier Testar; Olarte, Antonio Zorzano; Prieto, Manuel Palacin; Palomera, Fernando Albericio; Font, Francesc Yraola; Mian, Alec
Patent: US2007/66682 A1, 2007 ;
Location in patent: Page/Page column 17 ;
反应条件
1: 51 percent / SOCl2 / diethyl ether / Heating
2: 92 percent / KOH / tetrahydrofuran; H2O / Ambient temperature
View Scheme
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2973 - 2978
反应条件
1: 51 percent / SOCl2 / diethyl ether / Heating
2: 92 percent / KOH / tetrahydrofuran; H2O / Ambient temperature
3: 95 percent / diphenyl ether / 0.5 h / 240 - 250 °C
View Scheme
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2973 - 2978
反应条件
1: 51 percent / SOCl2 / diethyl ether / Heating
2: 92 percent / KOH / tetrahydrofuran; H2O / Ambient temperature
3: 95 percent / diphenyl ether / 0.5 h / 240 - 250 °C
4: 90 percent / aq. NaOH / methanol / Heating
View Scheme
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2973 - 2978
反应条件
1: 51 percent / SOCl2 / diethyl ether / Heating
2: 92 percent / KOH / tetrahydrofuran; H2O / Ambient temperature
3: 95 percent / diphenyl ether / 0.5 h / 240 - 250 °C
4: 90 percent / aq. NaOH / methanol / Heating
5: 87 percent
View Scheme
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2973 - 2978
