N-苄氧羰基-DL-正缬氨酸合成路线 (共 5 条)
反应条件
1: With sodium hydrogencarbonate in water T=0 - 20°C; 24.75 h; Inert atmosphere; 2: With hydrogenchloride in water pH=1;
参考文献
King, Amber M.; Salome, Christophe; Dinsmore, Jason; Salome-Grosjean, Elise; De Ryck, Marc; Kaminski, Rafal; Valade, Anne; Kohn, Harold
Journal of Medicinal Chemistry, 2011 , vol. 54, # 13 p. 4815 - 4830
反应条件
sodium hydroxide; benzyl chloroformate
参考文献
Kutscherow; Dorochowa
Zhurnal Obshchei Khimii, 1951 , vol. 21, p. 1486,1488; engl. Ausg. S. 1621, 1623
反应条件
citrate buffer; dl-cysteine hydrochloride; papain T=50°C; 24 h;
参考文献
Moriniere, J. L.; Danree, B.; Lemoine, J.; Guy, A.
Synthetic Communications, 1988 , vol. 18, # 4 p. 441 - 444
反应条件
resolved on CSP cellulose tris(3,5-dimethylphenylcarbamate) by chiral HPLC;
参考文献
Okamoto, Yoshio; Aburatani, Ryo; Kaida, Yuriko; Hatada, Koichi
Chemistry Letters, 1988 , p. 1125 - 1128
反应条件
resolved on CSP cellulose tris(3,5-dimethylphenylcarbamate) by chiral HPLC;
参考文献
Okamoto, Yoshio; Aburatani, Ryo; Kaida, Yuriko; Hatada, Koichi
Chemistry Letters, 1988 , p. 1125 - 1128