hydrogen; Ru2Cl4-(S)-(2,2'-bis(diphenylphosphino)-1,1'-binaphthyl)2*NEt3 in dichloromethane
T=50°C; P=76000 Torr; Title compound not separated from byproducts;
1: 2 h / heated on a steam bath
2: 3 h / heated on a steam bath
3: PCl5 / diethyl ether
View Scheme
参考文献
Hassall, Cedric H.; Kroehn, Antonin; Moody, Cristopher J.; Thomas, W. Anthony
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 155 - 164