in toluene
byproducts: tetraphenylantimony chloride; mixt. of Sb and Sn deriv. was allowed to stand in an evacuated glass ampooule at room temp. for 24 h; crystals of Ph4SbCl filtered off, filtrate evapd., residue chromd. on SiO2; identified by elem. anal. and NMR spectrum;
参考文献
Sharutin; Sharutina; Senchurin; Kovaleva; Shcherbakov; Gladyshev
Russian Journal of General Chemistry, 2000 , vol. 70, # 1 p. 64 - 65
in toluene
mixt. of Sb and Sn deriv. was allowed to stand in an evacuated glass ampoule at room temp. for 24 h; crystals of Ph4SbCl filtered off; filtrate evapd; residue chromd. on SiO2; identified by elem. anal.;
参考文献
Sharutin; Sharutina; Senchurin; Kovaleva; Shcherbakov; Gladyshev
Russian Journal of General Chemistry, 2000 , vol. 70, # 1 p. 64 - 65
