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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯基乙炔基三甲基硅烷
合成路线
（共 409 条）
2170-06-1
苯基乙炔基三甲基硅烷
→
反应条件
22057-84-7
反应条件
1: HAl(Bui)2 2: bis(dibenzylideneacetone)palladium(0) / acetonitrile / 25 °C View Scheme
参考文献
Ikenaga, Kazutoshi; Kikukawa, Kiyoshi; Matsuda, Tsutomu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1959 - 1964
5271-67-0
2-噻吩甲酰氯
+
2170-06-1
苯基乙炔基三甲基硅烷
→
反应条件
21985-04-6
反应条件
anhydrous iron chloride in nitromethane T=-15°C; 6 h; Inert atmosphereSeal tube;
参考文献
Gandeepan, Parthasarathy; Parthasarathy, Kanniyappan; Su, Tsu-Hui; Cheng, Chien-Hong
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 457 - 468
2170-06-1
苯基乙炔基三甲基硅烷
→
反应条件
21985-04-6
反应条件
1: methanol; potassium hydroxide / water / 12 h / 0 - 25 °C / Darkness; Inert atmosphere 2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 2 h / 25 °C / Inert atmosphere View Scheme
参考文献
Teiber, Marco; Mueller, Thomas J. J.
Chemical Communications, 2012 , vol. 48, # 15 p. 2080 - 2082
2170-06-1
苯基乙炔基三甲基硅烷
→
反应条件
2989-63-1
反应条件
1: potassium carbonate / methanol; dichloromethane 2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 20 °C / |Inert atmosphere 3: dichloro bis(acetonitrile) palladium(II) / acetonitrile / 86 °C / |Inert atmosphere 4: indium(III) chloride / acetonitrile / 3 h / |Reflux; |Inert atmosphere View Scheme
参考文献
Najahi, Ennaji; Valentin, Alexis; Fabre, Paul-Louis; Reybier, Karine; Nepveu, Francoise
European Journal of Medicinal Chemistry, 2014 , vol. 78, p. 269 - 274
4028-63-1
2,4,6-三甲基碘苯
+
2170-06-1
苯基乙炔基三甲基硅烷
→
反应条件
29778-31-2
反应条件
KOC(O)Ph; triphenylphosphine; copper(l) chloride in 1,3-dimethyl-imidazolidin-2-one T=120°C; Sila-Sonogashira-Hagihara cross-coupling reaction; 12 h; Inert atmosphere;
参考文献
Ihara, Hideki; Ueda, Akinori; Suginome, Michinori
Chemistry Letters, 2011 , vol. 40, # 9 p. 972 - 974
576-83-0
2-溴-1,3,5-三甲基苯
+
2170-06-1
苯基乙炔基三甲基硅烷
→
反应条件
29778-31-2
反应条件
copper(l) chloride; palladium dichloride; tris(p-fluoro phenyl)phosphine in N,N-dimethyl-formamide T=100°C; sila-Sonogashira-Hagihara cross-coupling; 12 h; Inert atmosphere;
参考文献
Nishihara, Yasushi; Inoue, Eiji; Noyori, Shintaro; Ogawa, Daisuke; Okada, Yoshiaki; Iwasaki, Masayuki; Takagi, Kentaro
Tetrahedron, 2012 , vol. 68, # 24 p. 4869 - 4881
3058-39-7
4-碘氰基苯
+
2170-06-1
苯基乙炔基三甲基硅烷
→
反应条件
29822-79-5
4-(2-苯基-1-乙炔)苯甲腈
反应条件
tetrakis(triphenylphosphine) palladium(0); copper(l) chloride in N,N-dimethyl-formamide T=80°C; sila-Sonogashira reaction; 1 h;
参考文献
Nishihara, Yasushi; Inoue, Eiji; Noyori, Shintaro; Ogawa, Daisuke; Okada, Yoshiaki; Iwasaki, Masayuki; Takagi, Kentaro
Tetrahedron, 2012 , vol. 68, # 24 p. 4869 - 4881
623-03-0
对氯苯甲腈
+
2170-06-1
苯基乙炔基三甲基硅烷
→
反应条件
29822-79-5
4-(2-苯基-1-乙炔)苯甲腈
反应条件
(4R,5R)-DIOP; palladium diacetate; copper(l) chloride in N,N-dimethyl-formamide T=20 - 120°C; Sila-Sonogashira cross-coupling reaction;
参考文献
Nishihara, Yasushi; Inoue, Eiji; Noyori, Shintaro; Ogawa, Daisuke; Okada, Yoshiaki; Iwasaki, Masayuki; Takagi, Kentaro
Tetrahedron, 2012 , vol. 68, # 24 p. 4869 - 4881
→
反应条件
29822-79-5
4-(2-苯基-1-乙炔)苯甲腈
反应条件
copper(l) chloride; palladium dichloride; tris(p-fluoro phenyl)phosphine in N,N-dimethyl-formamide T=100°C; sila-Sonogashira-Hagihara cross-coupling; 12 h; Inert atmosphere;
参考文献
Nishihara, Yasushi; Inoue, Eiji; Noyori, Shintaro; Ogawa, Daisuke; Okada, Yoshiaki; Iwasaki, Masayuki; Takagi, Kentaro
Tetrahedron, 2012 , vol. 68, # 24 p. 4869 - 4881
3058-39-7
4-碘氰基苯
+
2170-06-1
苯基乙炔基三甲基硅烷
→
反应条件
886-66-8
1,4-二苯基丁二炔
+
29822-79-5
4-(2-苯基-1-乙炔)苯甲腈
反应条件
anhydrous copper acetate in 1,3-dimethyl-imidazolidin-2-one T=120°C; 12 h; Inert atmosphere;
参考文献
Ihara, Hideki; Ueda, Akinori; Suginome, Michinori
Chemistry Letters, 2011 , vol. 40, # 9 p. 972 - 974
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