aluminium trichloride in dichloromethane
1.) -70 deg C, 60 min, 2.) -70 deg C -> room temperature;
参考文献
Jackson, Richard F. W.; Raphael, Ralph A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 535 - 539
1.1: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 0.92 h / |Inert atmosphere
1.2: 1 h
1.3: 0.75 h
2.1: potassium carbonate / o-di-fluorobenzene / 0.75 h
2.2: 20 °C / |Darkness; |Inert atmosphere; |Reflux
View Scheme
参考文献
Dixon, Luke I.; Carroll, Michael A.; Gregson, Thomas J.; Ellames, George J.; Harrington, Ross W.; Clegg, William
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 35 p. 5877 - 5884
