反应条件
1: 1.) DIBAL-H, 2.) N-bromosuccimide / 1.) hexane, RT, 20 h, 2.) hexane, from -20 deg C to RT, 3 h
2: 1.) n-BuLi / 1.) diethyl ether, reflux, 2 h, 2.) diethyl ether, from 0 deg C to RT
3: tetrabutylammonium fluoride (TBAF), H2O / tetrahydrofuran / 2 h / 60 °C
View Scheme
参考文献
Kurita, Jyoji; Ishii, Makoto; Yasuike, Shuji; Tsuchiya, Takashi
Journal of the Chemical Society, Chemical Communications, 1993 , # 17 p. 1309 - 1310
