1,3-苯并二氧戊环-2-酮合成路线 (共 25 条)
反应条件
palladium diacetate; triethylamine; triphenylphosphine in tetrahydrofuran T=100 - 110°C; P=20686.5 Torr; 15 h; Autoclave;
参考文献
Troisi, Luigino; Granito, Catia; Perrone, Serena; Rosato, Francesca
Tetrahedron Letters, 2011 , vol. 52, # 33 p. 4330 - 4332
反应条件
sodium hydroxide in chloroform T=61°C; 1.5 h; Inert atmosphere;
参考文献
US2010/123097 A1, ;
Page/Page column 8 ;
反应条件
di-tert-butyl peroxide in benzene T=140°C; 5 h;
参考文献
Sokolovskii, A. V.; Nazarov, D. V.; Rol'nik, L. Z.; Zlot-skii, S. S.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 6 p. 1305 - 1308,1159 - 1162
反应条件
di-tert-butyl peroxide in benzene T=140°C; 5 h;
参考文献
Sokolovskii, A. V.; Nazarov, D. V.; Rol'nik, L. Z.; Zlot-skii, S. S.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 6 p. 1305 - 1308,1159 - 1162
参考文献
Kaupp, Gerd; Boy, Juergen; Schmeyers, Jens
Advanced Synthesis and Catalysis, 1998 , vol. 340, # 4 p. 346 - 355
反应条件
hydrogen fluoride in various solvent(s) P=19501.6 Torr; 6 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 63, # 8 p. 2493 - 2496
反应条件
di-tert-butyl peroxide in chlorobenzene T=140°C; Yield given;
参考文献
Doklady Chemistry, , vol. 271, p. 266 - 269
Dokl. Akad. Nauk SSSR Ser. Khim., , vol. 271, # 6 p. 1395 - 1398
反应条件
sodium hydride in tetrahydrofuran
参考文献
Journal of Organic Chemistry, , vol. 41, p. 2039 - 2042
反应条件
1: benzene; diethyl ether 2: NaH / tetrahydrofuran View Scheme
参考文献
Journal of Organic Chemistry, , vol. 41, p. 2039 - 2042
参考文献
Gross; Keitel; Costisella
Acta Chimica Hungarica, 1984 , vol. 116, # 3 p. 229 - 233