N-羟基-5-降冰片烯-2,3-二甲酰亚胺合成路线 （共 19 条）
反应条件
1: 1.) NaOH / 1.) MeOH; 2.) benzene, 10-15 deg C, 2 h 2: pyridine / 1.) room temp., 1 h; 2.) 35 deg C, 3 h 3: 85 percent / tertiary amine / H2O; dioxane / 3 h View Scheme
参考文献
Henklein, Peter; Heyne, Hans-Ulrich; Halatsch, Wolf-Rainer; Niedrich, Hartmut
Synthesis, 1987 , # 2 p. 166 - 167
反应条件
1: 1.) NaOH / 1.) MeOH; 2.) benzene, 10-15 deg C, 2 h 2: pyridine / 1.) room temp., 1 h; 2.) 35 deg C, 3 h 3: 64 percent / tertiary amine / H2O; dioxane / 3 h View Scheme
参考文献
Henklein, Peter; Heyne, Hans-Ulrich; Halatsch, Wolf-Rainer; Niedrich, Hartmut
Synthesis, 1987 , # 2 p. 166 - 167
反应条件
1: 1.) NaOH / 1.) MeOH; 2.) benzene, 10-15 deg C, 2 h 2: pyridine / 1.) room temp., 1 h; 2.) 35 deg C, 3 h 3: 81 percent / tertiary amine / H2O; dioxane / 3 h View Scheme
参考文献
Henklein, Peter; Heyne, Hans-Ulrich; Halatsch, Wolf-Rainer; Niedrich, Hartmut
Synthesis, 1987 , # 2 p. 166 - 167
反应条件
triethylamine in N,N-dimethyl-formamide
18 h;
参考文献
Amlaiky, Nourdine; Leclerc, Gerard; Carpy, Alain
Journal of Organic Chemistry, 1982 , vol. 47, # 3 p. 517 - 523
反应条件
sodium hydroxide
1.) MeOH; 2.) benzene, 10-15 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Henklein, Peter; Halatsch, Wolf-Rainer; Heyne, Hans-Ulrich
Zeitschrift fuer Chemie (Stuttgart, Germany), 1986 , vol. 26, # 9 p. 329 - 330
反应条件
1: Heating
2: 83 percent / tetrahydrofuran / 0 °C
View Scheme
参考文献
Henklein, Peter; Halatsch, Wolf-Rainer; Heyne, Hans-Ulrich
Zeitschrift fuer Chemie (Stuttgart, Germany), 1986 , vol. 26, # 9 p. 329 - 330
反应条件
triethylamine in dichloromethane
1 h;
参考文献
Matsueda, Rei; Kaiser, Emil Thomas
Heterocycles, 1981 , vol. 15, # 2 p. 1089 - 1092
反应条件
1: 1.) NaOH / 1.) MeOH; 2.) benzene, 10-15 deg C, 2 h
2: pyridine / 1.) room temp., 1 h; 2.) 35 deg C, 3 h
View Scheme
参考文献
Henklein, Peter; Heyne, Hans-Ulrich; Halatsch, Wolf-Rainer; Niedrich, Hartmut
Synthesis, 1987 , # 2 p. 166 - 167
参考文献
Bauer; Miarka
Journal of Organic Chemistry, 1959 , vol. 24, p. 1293,1295
