6,7-二甲氧基-1,2-二氢异喹啉-3(4H)-酮合成路线 （共 11 条）
反应条件
ammonia in ethanol T=25°C; 0.166667 h;
参考文献
White, Emil H.; Jelinski, Lynn W.; Politzer, Ieva R.; Branchini, Bruce R.; Roswell, David F.
Journal of the American Chemical Society, 1981 , vol. 103, # 14 p. 4231 - 4239
参考文献
White, Emil H.; Jelinski, Lynn W.; Politzer, Ieva R.; Branchini, Bruce R.; Roswell, David F.
Journal of the American Chemical Society, 1981 , vol. 103, # 14 p. 4231 - 4239
反应条件
1: 66 percent / HCl, HOAc 2: HBr 3: 20 percent / ammonia gas / ethanol / 0.17 h / 25 °C View Scheme
参考文献
White, Emil H.; Jelinski, Lynn W.; Politzer, Ieva R.; Branchini, Bruce R.; Roswell, David F.
Journal of the American Chemical Society, 1981 , vol. 103, # 14 p. 4231 - 4239
反应条件
T=300 - 306°C; P=20 Torr;
参考文献
Watanabe, Yasuo; Kamochi, Yasoko; Miyazaki, Tokumitsu
Heterocycles, 1981 , vol. 16, # 4 p. 609 - 611
反应条件
1: 68 percent / Cs2CO3; molecular sieves 4 Angstroem / dimethylformamide / 14 h / 0 - 20 °C 2: 2,6-di-O-methyl-β-cyclodextrin; sodium phosphate buffer; penicillin G acylase (EC 3.5.1.11) immobilized on Eupergit C / acetone / 48 h / 37 °C / pH 7.0 View Scheme
参考文献
Grether, Uwe; Waldmann, Herbert
Chemistry - A European Journal, 2001 , vol. 7, # 5 p. 959 - 971
反应条件
in acetic acid; trifluoroacetic acid Pictet-Spengler reaction; 1 h; Heating;
参考文献
Ivanov, Iliyan; Venkov, Atanas
Heterocycles, 2001 , vol. 55, # 8 p. 1569 - 1580
反应条件
AlCl3, aluminium chloride in diethyl ether 6 h; regioselective reaction;
参考文献
Quevedo, Rodolfo; Baquero, Edwin; Rodriguez, Mario
Tetrahedron Letters, 2010 , vol. 51, # 13 p. 1774 - 1778
反应条件
phosphoric acid in ethyl acetate 1 h; Heating;
参考文献
Kamochi, Yasuko; Watanabe, Yasuo
Heterocycles, 1987 , vol. 26, # 9 p. 2385 - 2391
反应条件
(S)-pyrophosphoric acid 14 h; Ambient temperature;
参考文献
Watanabe, Yasuo; Kamochi, Yasoko; Miyazaki, Tokumitsu
Heterocycles, 1981 , vol. 16, # 4 p. 609 - 611
反应条件
(S)-pyrophosphoric acid 12 h; Ambient temperature;
参考文献
Kamochi, Yasuko; Watanabe, Yasuo
Heterocycles, 1987 , vol. 26, # 9 p. 2385 - 2391
