三氟甲烷磺酸3-甲氧基-2-(三甲基硅基)苯酯合成路线 (共 39 条)
反应条件
2: LDA 3: nBuLi View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 37, # 19 p. 2659 - 2661
反应条件
1: LDA 2: nBuLi View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 37, # 19 p. 2659 - 2661
参考文献
Angewandte Chemie - International Edition, , vol. 37, # 19 p. 2659 - 2661
反应条件
cesium fluoride in acetonitrile T=20°C; 24 h;
参考文献
Liu, Zhijian; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 8 p. 3198 - 3209
反应条件
1: With tetrabutyl ammonium fluoride T=20°C; 3 h; Inert atmosphere; 2: With water
参考文献
Yoshioka, Eito; Miyabe, Hideto
Tetrahedron, 2012 , vol. 68, # 1 p. 179 - 189
反应条件
1: CsF / acetonitrile / 10 h / 20 °C 2: tricyclohexylphosphine / Pd(OAc)2 / acetonitrile / 24 h / 100 °C View Scheme
参考文献
Liu, Zhijian; Larock, Richard C.
Tetrahedron, 2007 , vol. 63, # 2 p. 347 - 355
反应条件
methyl-3-phenyl-2-propynoate; cesium fluoride T=25°C; 1 h; Inert atmosphere; Reagent/catalyst;
参考文献
Tetrahedron Letters, , vol. 55, # 8 p. 1402 - 1405
反应条件
1: N,N-dimethyl-formamide; 3-methoxy-2-(trimethylsilyl)phenyl-trifluoromethanesulfonate With cesium fluoride T=20°C; 0.25 h; Inert atmosphere; 2: triethyl borane T=20°C; 12 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 12, # 9 p. 1956 - 1959
反应条件
cesium fluoride T=20°C; 12 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 15, # 15 p. 3938 - 3941
反应条件
tetrabutyl ammonium fluoride T=20°C; 12 h; Inert atmosphere; regioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 29 p. 6638 - 6642