三氟甲烷磺酸3-甲氧基-2-(三甲基硅基)苯酯合成路线 （共 39 条）
反应条件
1: With tetrabutyl ammonium fluoride in acetonitrile T=20°C; 3 h; Inert atmosphere; 2: With water T=20°C;
参考文献
Tetrahedron, , vol. 68, # 1 p. 179 - 189
反应条件
cesium fluoride in acetonitrile T=20°C; 6 h;
参考文献
Rao, U. Narasimha; Sathunuru, Ramadas; Biehl, Edward R.
Heterocycles, 2004 , vol. 63, # 5 p. 1067 - 1075
反应条件
1: With tetrabutyl ammonium fluoride T=20°C; 3 h; Inert atmosphere; 2: With water T=20°C;
参考文献
Tetrahedron, , vol. 68, # 1 p. 179 - 189
反应条件
1: 3-methoxy-2-(trimethylsilyl)phenyl-trifluoromethanesulfonate With N,N-dimethyl-thioformamide; tetrabutyl ammonium fluoride in acetonitrile
T=20°C; 3 h; Inert atmosphere;
2: acetic anhydride in acetonitrile
T=20°C; 12 h;
参考文献
Yoshioka, Eito; Miyabe, Hideto
Tetrahedron, 2012 , vol. 68, # 1 p. 179 - 189
反应条件
TBAHF2
T=20°C; 3 h; Inert atmosphere; regioselective reaction;
参考文献
Yoshioka, Eito; Kohtani, Shigeru; Miyabe, Hideto
Angewandte Chemie - International Edition, 2011 , vol. 50, # 29 p. 6638 - 6642
反应条件
tetrabutyl ammonium fluoride
T=20°C; 12 h; Inert atmosphere; regioselective reaction;
参考文献
Yoshioka, Eito; Kohtani, Shigeru; Miyabe, Hideto
Angewandte Chemie - International Edition, 2011 , vol. 50, # 29 p. 6638 - 6642
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=-78 - 20°C; 20 h;
参考文献
Liu, Zhijian; Shi, Feng; Martinez, Pablo D. G.; Raminelli, Cristiano; Larock, Richard C.
Journal of Organic Chemistry, 2008 , vol. 73, # 1 p. 219 - 226
反应条件
cesium fluoride in tetrahydrofuran
T=90°C; 24 h;
参考文献
Zhao, Jian; Larock, Richard C.
Organic Letters, 2005 , vol. 7, # 19 p. 4273 - 4275
Title/Abstract Full Text View citing articles Show Details
Zhao, Jian; Larock, Richard C.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 583 - 588
反应条件
cesium fluoride in acetonitrile
T=20°C; 5 h;
参考文献
Liu, Zhijian; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 8 p. 3198 - 3209
反应条件
cesium fluoride in acetonitrile
48 h;
参考文献
ASTRAZENECA AB; ASTEX THERAPEUTICS LTD
Patent: WO2007/58602 A2, 2007 ;
Location in patent: Page/Page column 193-194 ;
WO 2007/058602 A2
