三氟甲烷磺酸3-甲氧基-2-(三甲基硅基)苯酯合成路线 （共 39 条）
反应条件
cesium fluoride; tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium(0) in toluene; acetonitrile
T=110°C; 12 h;
参考文献
Zhang, Xiaoxia; Larock, Richard C.
Organic Letters, 2005 , vol. 7, # 18 p. 3973 - 3976
反应条件
cesium fluoride; tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium(0) in toluene; acetonitrile
T=110°C; 12 h;
参考文献
Zhang, Xiaoxia; Larock, Richard C.
Organic Letters, 2005 , vol. 7, # 18 p. 3973 - 3976
反应条件
1: With tetrabutyl ammonium fluoride in acetonitrile
T=20°C; 3 h; Inert atmosphere;
2: With water
T=20°C;
参考文献
Yoshioka, Eito; Miyabe, Hideto
Tetrahedron, 2012 , vol. 68, # 1 p. 179 - 189
反应条件
copper(l) iodide; cesium fluoride in toluene; acetonitrile
T=150°C; 0.5 h; Inert atmosphereMicrowave irradiation;
参考文献
Akubathini, Shashidhar Kumar; Biehl, Ed
Tetrahedron Letters, 2009 , vol. 50, # 16 p. 1809 - 1811
反应条件
1: diethylzinc; tetrabutyl ammonium fluoride / 12 h / -60 - 20 °C / |Inert atmosphere
2: diethylzinc / tetrahydrofuran / 3 h / -60 - 20 °C
View Scheme
参考文献
Yoshioka, Eito; Tanaka, Hidekazu; Kohtani, Shigeru; Miyabe, Hideto
Organic Letters, 2013 , vol. 15, # 15 p. 3938 - 3941
反应条件
tetrabutyl ammonium fluoride; diethylzinc
T=-60 - 20°C; 12 h; Inert atmosphere;
参考文献
Yoshioka, Eito; Tanaka, Hidekazu; Kohtani, Shigeru; Miyabe, Hideto
Organic Letters, 2013 , vol. 15, # 15 p. 3938 - 3941
反应条件
cesium fluoride; dodecacarbonyl tetracobalt in acetonitrile
T=60°C; P=7600.51 Torr; 12 h; Title compound not separated from byproducts.;
参考文献
Chatani; Kamitani; Oshita; Fukumoto; Murai
Journal of the American Chemical Society, 2001 , vol. 123, # 50 p. 12686 - 12687
反应条件
cesium fluoride; dodecacarbonyl tetracobalt in acetonitrile
T=60°C; P=7600.51 Torr; 12 h; Title compound not separated from byproducts.;
参考文献
Chatani; Kamitani; Oshita; Fukumoto; Murai
Journal of the American Chemical Society, 2001 , vol. 123, # 50 p. 12686 - 12687
反应条件
copper(l) iodide; cesium fluoride in toluene; acetonitrile
T=150°C; 0.5 h; Inert atmosphereMicrowave irradiation;
参考文献
Akubathini, Shashidhar Kumar; Biehl, Ed
Tetrahedron Letters, 2009 , vol. 50, # 16 p. 1809 - 1811
