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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
217962-06-6
合成路线
（共 12 条）
362690-25-3
→
反应条件
217962-06-6
反应条件
sodium methylate in methanol Heating;
参考文献
Belle; Bougault; Averbuch; Durif; Pierre; Latour; Le Pape
Journal of the American Chemical Society, 2001 , vol. 123, # 33 p. 8053 - 8066
181118-26-3
→
反应条件
217962-06-6
反应条件
1: 80 percent / PBr3 / diethyl ether / 3 h / 20 °C 2: 59 percent / Et3N / ethyl acetate / 72 h 3: NaOMe / methanol / Heating View Scheme
参考文献
Belle; Bougault; Averbuch; Durif; Pierre; Latour; Le Pape
Journal of the American Chemical Society, 2001 , vol. 123, # 33 p. 8053 - 8066
41907-41-9
→
反应条件
217962-06-6
反应条件
1.1: Et3N / tetrahydrofuran / 1 h / -5 °C 2.1: 396 mg / aq. NaBH4 / tetrahydrofuran / 12 h / 20 °C 3.1: 97 percent / MnO2 / CH2Cl2 / 2 h / Heating 4.1: methanol / 2 h / Heating 4.2: 98 percent / NaBH4 / methanol / 12 h 5.1: 75 percent / NaBH3CN; AcOH / methanol / 72 h 6.1: 200 mg / t-BuOK / tetrahydrofuran / 2 h View Scheme
参考文献
Belle; Bougault; Averbuch; Durif; Pierre; Latour; Le Pape
Journal of the American Chemical Society, 2001 , vol. 123, # 33 p. 8053 - 8066
147-93-3
硫代水杨酸
→
反应条件
217962-06-6
反应条件
1.1: NaH / tetrahydrofuran / 1 h / 20 °C 1.2: 95 percent / tetrahydrofuran / 12 h / Heating 2.1: Et3N / tetrahydrofuran / 1 h / -5 °C 3.1: 396 mg / aq. NaBH4 / tetrahydrofuran / 12 h / 20 °C 4.1: 97 percent / MnO2 / CH2Cl2 / 2 h / Heating 5.1: methanol / 2 h / Heating 5.2: 98 percent / NaBH4 / methanol / 12 h 6.1: 75 percent / NaBH3CN; AcOH / methanol / 72 h 7.1: 200 mg / t-BuOK / tetrahydrofuran / 2 h View Scheme
参考文献
Belle; Bougault; Averbuch; Durif; Pierre; Latour; Le Pape
Journal of the American Chemical Society, 2001 , vol. 123, # 33 p. 8053 - 8066
181118-27-4
→
反应条件
217962-06-6
反应条件
1.1: methanol / 2 h / Heating 1.2: 98 percent / NaBH4 / methanol / 12 h 2.1: 75 percent / NaBH3CN; AcOH / methanol / 72 h 3.1: 200 mg / t-BuOK / tetrahydrofuran / 2 h View Scheme
参考文献
Belle; Bougault; Averbuch; Durif; Pierre; Latour; Le Pape
Journal of the American Chemical Society, 2001 , vol. 123, # 33 p. 8053 - 8066
362690-24-2
→
反应条件
217962-06-6
反应条件
1: 75 percent / NaBH3CN; AcOH / methanol / 72 h 2: 200 mg / t-BuOK / tetrahydrofuran / 2 h View Scheme
参考文献
Belle; Bougault; Averbuch; Durif; Pierre; Latour; Le Pape
Journal of the American Chemical Society, 2001 , vol. 123, # 33 p. 8053 - 8066
870993-08-1
→
反应条件
217962-06-6
反应条件
1: 59 percent / Et3N / ethyl acetate / 72 h 2: NaOMe / methanol / Heating View Scheme
参考文献
Thapper, Anders; Behrens, Axel; Fryxelius, Jacob; Johansson, Maria H.; Prestopino, Fabio; Czaun, Miklos; Rehder, Dieter; Nordlander, Ebbe
Dalton Transactions, 2005 , # 21 p. 3566 - 3571
1121-60-4
吡啶-2-甲醛
→
反应条件
217962-06-6
反应条件
1.1: ethanol / 0.25 h 1.2: 86 percent / NaBH4 / ethanol / 0.83 h / Heating 2.1: KOH / H2O 3.1: 59 percent / Et3N / ethyl acetate / 72 h 4.1: NaOMe / methanol / Heating View Scheme
参考文献
Thapper, Anders; Behrens, Axel; Fryxelius, Jacob; Johansson, Maria H.; Prestopino, Fabio; Czaun, Miklos; Rehder, Dieter; Nordlander, Ebbe
Dalton Transactions, 2005 , # 21 p. 3566 - 3571
3731-51-9
2-氨甲基吡啶
→
反应条件
217962-06-6
反应条件
1.1: ethanol / 0.25 h 1.2: 86 percent / NaBH4 / ethanol / 0.83 h / Heating 2.1: KOH / H2O 3.1: 59 percent / Et3N / ethyl acetate / 72 h 4.1: NaOMe / methanol / Heating View Scheme
参考文献
Thapper, Anders; Behrens, Axel; Fryxelius, Jacob; Johansson, Maria H.; Prestopino, Fabio; Czaun, Miklos; Rehder, Dieter; Nordlander, Ebbe
Dalton Transactions, 2005 , # 21 p. 3566 - 3571
4521-31-7
2-巯基苯甲醇
→
反应条件
217962-06-6
反应条件
1: 86 percent / NaOH / ethanol; H2O / 5 h 2: 80 percent / PBr3 / diethyl ether / 3 h / 20 °C 3: 59 percent / Et3N / ethyl acetate / 72 h 4: NaOMe / methanol / Heating View Scheme
参考文献
Thapper, Anders; Behrens, Axel; Fryxelius, Jacob; Johansson, Maria H.; Prestopino, Fabio; Czaun, Miklos; Rehder, Dieter; Nordlander, Ebbe
Dalton Transactions, 2005 , # 21 p. 3566 - 3571
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