(甲氧基羰基甲基)三苯基氯化鏻合成路线 （共 28 条）
反应条件
chloro-diphenylphosphine in benzene
参考文献
Justus Liebigs Annalen der Chemie, , vol. 699, p. 40 - 52
参考文献
Doleschall, Gabor
Synthesis, 1981 , # 6 p. 478 - 480
参考文献
Doleschall, Gabor
Synthesis, 1981 , # 6 p. 478 - 480
反应条件
in dichloromethane Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent;
参考文献
Inorganic Chemistry, , vol. 40, # 7 p. 1683 - 1689
反应条件
in dichloromethane byproducts: DMSO; Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent;
参考文献
Inorganic Chemistry, , vol. 40, # 7 p. 1683 - 1689
反应条件
in dichloromethane Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent; elem. anal.;
参考文献
Inorganic Chemistry, , vol. 40, # 7 p. 1683 - 1689
反应条件
in dichloromethane Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent; elem. anal.;
参考文献
Inorganic Chemistry, , vol. 40, # 7 p. 1683 - 1689
反应条件
in dichloromethane Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent; elem. anal.;
参考文献
Inorganic Chemistry, , vol. 40, # 7 p. 1683 - 1689
反应条件
in dichloromethane Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent; elem. anal.;
参考文献
Inorganic Chemistry, , vol. 40, # 7 p. 1683 - 1689
反应条件
in dichloromethane Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent; elem. anal.;
参考文献
Inorganic Chemistry, , vol. 40, # 7 p. 1683 - 1689
