N-苄基-1,3-苯并噻唑-2-胺合成路线 （共 21 条）
反应条件
1,10-phenanthroline; caesium carbonate; copper(l) iodide in ethylene glycol dimethyl ether
T=80°C;
参考文献
Joyce, Laurie L.; Evindar, Ghotas; Batey, Robert A.
Chemical Communications, 2004 , # 4 p. 446 - 447
反应条件
sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene in neat (no solvent)
T=20°C; Green chemistry;
参考文献
Verma, Sanjeev K.; Acharya; Ghorpade, Ramarao; Pratap, Ajay; Kaushik
RSC Advances, 2013 , vol. 3, # 41 p. 18783 - 18786
反应条件
copper(l) iodide; tetrabutylammomium bromide; palladium dichloride in 1-methyl-pyrrolidin-2-one; dimethyl sulfoxide
T=100°C; 12 h; Inert atmosphere;
参考文献
Inamoto, Kiyofumi; Hasegawa, Chisa; Hiroya, Kou; Doi, Takayuki
Organic Letters, 2008 , vol. 10, # 22 p. 5147 - 5150
反应条件
1,10-phenanthroline; sodium hydrogencarbonate in water
T=80°C; 2 h;
参考文献
Zhang, Wu; Yue, Yun; Yu, Dan; Song, Lei; Xu, Yang-Yang; Tian, Yu-Jie; Guo, Yu-Jun
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 11-12 p. 2283 - 2287
参考文献
Fajkusova, Dagmar; Pesko, Matus; Keltosova, Stanislava; Guo, Jiahui; Oktabec, Zbynek; Vejsova, Marcela; Kollar, Peter; Coffey, Aidan; Csollei, Jozef; Kralova, Katarina; Jampilek, Josef
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 24 p. 7059 - 7068
反应条件
[{(η5-C5Me5)IrCl}2(μ-Cl)2]; sodium hydroxide
T=150°C; 12 h; Inert atmosphere; regioselective reaction;
参考文献
Li, Feng; Shan, Haixia; Chen, Lin; Kang, Qikai; Zou, Po
Chemical Communications, 2012 , vol. 48, # 4 p. 603 - 605
反应条件
copper(l) iodide; potassium carbonate in dimethyl sulfoxide
T=95°C; 24 h; Inert atmosphere;
参考文献
Shen, Guodong; Lv, Xin; Bao, Weiliang
European Journal of Organic Chemistry, 2009 , # 34 p. 5897 - 5901
反应条件
1: carbon disulfide; benzylamine With potassium carbonate in N,N-dimethyl-formamide
T=0°C; 1 h;
2: 2-iodo aniline With CuCl2·2H2O in N,N-dimethyl-formamide
T=110°C; 6 h;
参考文献
Ma, Dawei; Lu, Xu; Shi, Liu; Zhang, Hui; Jiang, Yongwen; Liu, Xiangqian
Angewandte Chemie - International Edition, 2011 , vol. 50, # 5 p. 1118 - 1121
反应条件
dipotassium peroxodisulfate; sodium acetate; [Co(O2CCH3)2]*4H2O in 1,4-dioxane
T=100°C; 18 h;
参考文献
Zhu, Tong-Hao; Wang, Shun-Yi; Wang, Gao-Nan; Ji, Shun-Jun
Chemistry - A European Journal, 2013 , vol. 19, # 19 p. 5850 - 5853
反应条件
1: acetonitrile / 1 h / 20 °C
2: 100 percent / Cs2CO3; 1,10-phenanthroline / CuI / 1,2-dimethoxy-ethane / 80 °C
View Scheme
参考文献
Joyce, Laurie L.; Evindar, Ghotas; Batey, Robert A.
Chemical Communications, 2004 , # 4 p. 446 - 447
