1,3,5-三苯基-1H-吡唑合成路线 (共 78 条)
反应条件
iodine in water
T=60°C; Green chemistry; SolventReagent/catalyst;
参考文献
Rai, Pratibha; Srivastava, Madhulika; Singh, Jagdamba; Singh, Jaya
RSC Advances, 2014 , vol. 4, # 2 p. 779 - 783
反应条件
triethylamine in methanol
P=760.051 Torr; 6 h; Schlenk technique; Reagent/catalyst;
参考文献
Li, Zelong; Liu, Jianhua; Huang, Zhiwei; Yang, Ying; Xia, Chungu; Li, Fuwei
ACS Catalysis, 2013 , vol. 3, # 5 p. 839 - 845
反应条件
copper(l) iodide; tri-tert-butyl phosphine; caesium carbonate; palladium diacetate in toluene; acetonitrile
T=80°C; 18 h;
参考文献
Stonehouse, Jeffrey P.; Chekmarev, Dmitriy S.; Ivanova, Natalya V.; Lang, Stuart; Pairaudeau, Garry; Smith, Neal; Stocks, Michael J.; Sviridov, Sergey I.; Utkina, Lyubov M.
Synlett, 2008 , # 1 p. 100 - 104
反应条件
copper(l) iodide; triethylamine in acetonitrile
T=82°C; 2 h; Inert atmosphere;
参考文献
Zora, Metin; Kivrak, Arif
Journal of Organic Chemistry, 2011 , vol. 76, # 22 p. 9379 - 9390
反应条件
palladium diacetate in anhydrous xylene
T=140°C; 22 h; Inert atmosphereSchlenk techniqueMolecular sieve;
参考文献
Smari, Imen; Youssef, Chiraz; Yuan, Kedong; Beladhria, Anissa; Ben Ammar, Hamed; Ben Hassine, Bechir; Doucet, Henri
European Journal of Organic Chemistry, 2014 , vol. 2014, # 8 p. 1778 - 1786
反应条件
in N,N-dimethyl-formamide
T=100°C; 5 h;
参考文献
Kovacs, Szabolcs; Novak, Zoltan
Tetrahedron, 2013 , vol. 69, # 43 p. 8987 - 8993
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane
T=20°C; 2 h; regioselective reaction;
参考文献
Desai, Vidya G.; Satardekar, Pooja C.; Polo, Sampada; Dhumaskar, Kashinath
Synthetic Communications, 2012 , vol. 42, # 6 p. 836 - 842
反应条件
copper(I) bromide dimethylsulfide complex; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium iodide in 1,2-dichloro-ethane
T=135°C; 5 h; Schlenk technique;
参考文献
Zhang, Guangwu; Zhao, Yan; Ge, Haibo
Angewandte Chemie - International Edition, 2013 , vol. 52, # 9 p. 2559 - 2563
Angew. Chem., 2013 , vol. 125, # 9 p. 2619 - 2623,5
参考文献
Moureu; Brachin
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1903 , vol. 136, p. 1264
Bulletin de la Societe Chimique de France, 1904 , vol. <3> 31, p. 172
反应条件
in toluene
T=90°C; 8 h;
参考文献
Barluenga, Jose; Lopez-Ortiz, J. Francisco; Tomas, Miguel; Gotor, Vicente
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1891 - 1895